methyl-stigmasteryl ether

Base Information

• Chemical Name: methyl-stigmasteryl ether
• CAS No.: 65556-64-1
• Molecular Formula: C₃₀H₅₀O
• Molecular Weight: 426.726

Synonyms:

Chemical Property of methyl-stigmasteryl ether

Chemical Property:

Purity/Quality:

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Technology Process of methyl-stigmasteryl ether

There total 6 articles about methyl-stigmasteryl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) → methyl-stigmasteryl ether (10453-25-5,65556-64-1) + methyl-(3α.5α-cyclo-stigmasten-(22t)-yl-(6β))-ether (53603-94-4,70832-49-4,108866-13-3,117467-15-9)

Guidance literature:

With potassium acetate;

DOI:10.1021/ja01869a022 DOI:10.1021/ja01200a035 DOI:10.1021/ja01243a007

Reference yield:

methanol (67-56-1) + butyl-(3α.5α-cyclo-stigmasten-(22t)-yl-(6β))-ether → methyl-stigmasteryl ether (10453-25-5,65556-64-1)

Guidance literature:

With sulfuric acid;

DOI:10.1021/ja01189a035

Reference yield:

methanol (67-56-1) → methyl-stigmasteryl ether (10453-25-5,65556-64-1)

Guidance literature:

upstream raw materials:

methanol

stigmasteryl tosylate

sodium acetate

sulfuric acid

Downstream raw materials:

(3S,4R,5R,8S,9S,10R,13R,14S,17R)-17-((1R,4S)-4-Ethyl-1,5-dimethyl-hexyl)-3-methoxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-4-ol

(3S,4R,8S,9S,10R,13R,14S,17R)-17-((E)-(1R,4R)-4-Ethyl-1,5-dimethyl-hex-2-enyl)-3-methoxy-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-4-ol

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