2-[5-(Benzyloxy)-2-bromophenyl]-2-methyloxirane

Base Information

Chemical Name:2-[5-(Benzyloxy)-2-bromophenyl]-2-methyloxirane
CAS No.:105805-17-2
Molecular Formula:C16H15BrO2
Molecular Weight:319.198
Hs Code.:
DSSTox Substance ID:DTXSID90556824

Synonyms:105805-17-2;2-[5-(Benzyloxy)-2-bromophenyl]-2-methyloxirane;DTXSID90556824

Suppliers and Price of 2-[5-(Benzyloxy)-2-bromophenyl]-2-methyloxirane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-[5-(Benzyloxy)-2-bromophenyl]-2-methyloxirane

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:318.02554
Heavy Atom Count:19
Complexity:303

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CO1)C2=C(C=CC(=C2)OCC3=CC=CC=C3)Br

Technology Process of 2-[5-(Benzyloxy)-2-bromophenyl]-2-methyloxirane

There total 5 articles about 2-[5-(Benzyloxy)-2-bromophenyl]-2-methyloxirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1774-47-6
trimethylsulfoxonium iodide

: 105805-16-1
1-[2-bromo-5-(phenylmethoxy)phenyl]ethanone

: 105805-17-2
2-(5'-benzyloxy-2'-bromophenyl)-2-methyl-oxirane

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; at 55 ℃; for 3h;

Reference yield: 94.0%

: 105805-16-1
1-[2-bromo-5-(phenylmethoxy)phenyl]ethanone

: 70775-39-2,5367-24-8
dimethylsulfoxonium methylide

: 105805-17-2
2-(5'-benzyloxy-2'-bromophenyl)-2-methyl-oxirane

Guidance literature:: In dimethyl sulfoxide; at 55 ℃;
DOI:10.1039/c39860001062

Reference yield:

: 34068-01-4
1-[3-(phenylmethoxy)phenyl]ethan-1-one

: 105805-17-2
2-(5'-benzyloxy-2'-bromophenyl)-2-methyl-oxirane

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / sodium acetate, bromine / acetic acid / 24 h / Ambient temperature; in the dark

2: 94 percent / sodium hydride / dimethylsulfoxide / 3 h / 55 °C

With bromine; sodium acetate; sodium hydride; In acetic acid; dimethyl sulfoxide;