phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranuric acid N-phenylamide

Base Information

Chemical Name:phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranuric acid N-phenylamide
CAS No.:926641-89-6
Molecular Formula:C₂₄H₂₅NO₉
Molecular Weight:471.464
Hs Code.:

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Chemical Property of phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranuric acid N-phenylamide

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Technology Process of phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranuric acid N-phenylamide

There total 4 articles about phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranuric acid N-phenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 926641-75-0
2,3,4-tri-O-acetyl-1,6-anhydro-6-Z-phenylimino-β-D-glucopyranose

: 1529-17-5
phenyltrimethylsilyl ether

: 2,3,4-tri-O-acetyl-D-glucopyranuronic acid phenylamide

: 926641-89-6
phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranuric acid N-phenylamide

Guidance literature:: With tin(IV) chloride; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/j.carres.2006.10.023

Reference yield:

: 926641-75-0
2,3,4-tri-O-acetyl-1,6-anhydro-6-Z-phenylimino-β-D-glucopyranose

: 108-95-2,27073-41-2
phenol

: 2,3,4-tri-O-acetyl-D-glucopyranuronic acid phenylamide

: 926641-89-6
phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranuric acid N-phenylamide

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; tin(IV) chloride; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.carres.2006.10.023

Reference yield:

: 926641-71-6
2,3,4-tri-O-acetyl-1-bromo-1-deoxy-α-D-glucopyranosiduronic acid N-phenylamide

: 926641-89-6
phenyl 2,3,4-tri-O-acetyl-β-D-glucopyranuric acid N-phenylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / AgClO₄; Ag₂CO₃ / CH₂Cl₂

2: 22 percent / SnCl₄ / CH₂Cl₂ / 24 h / 20 °C

With silver perchlorate; tin(IV) chloride; silver carbonate; In dichloromethane;
DOI:10.1016/j.carres.2006.10.023