p-bromophenacyl ester dextrorotatory α-(7-bromo-1-naphthyl)-propionic acid

Base Information

Chemical Name:p-bromophenacyl ester dextrorotatory α-(7-bromo-1-naphthyl)-propionic acid
CAS No.:77389-16-3
Molecular Formula:C₂₁H₁₆Br₂O₃
Molecular Weight:476.164
Hs Code.:

Synonyms:

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Chemical Property of p-bromophenacyl ester dextrorotatory α-(7-bromo-1-naphthyl)-propionic acid

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Technology Process of p-bromophenacyl ester dextrorotatory α-(7-bromo-1-naphthyl)-propionic acid

There total 13 articles about p-bromophenacyl ester dextrorotatory α-(7-bromo-1-naphthyl)-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32281-97-3
7-bromo-3,4-dihydro-2H-naphthalen-1-one

: 77389-16-3,77389-20-9
p-bromophenacyl ester α-(7-bromo-3,4-dihydro-1-naphthyl)-propionic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) zinc dust, iodine / 1.) benzene, 40 deg, , 2.) benzene, reflux, 2 h

2: 17 g / anhydrous formic acid / 0.5 h / Heating

3: 14 g / sulfur / 5 h / 198 - 200 °C

4: 6 g / aq. KOH / ethanol / 3 h / Heating

5: 1.8 g / methanol / 1 h / Heating

With potassium hydroxide; formic acid; iodine; sulfur; zinc; In methanol; ethanol;

Reference yield:

: 32281-97-3
7-bromo-3,4-dihydro-2H-naphthalen-1-one

: 77389-16-3,77389-20-9
p-bromophenacyl ester dextrorotatory α-(7-bromo-1-naphthyl)-propionic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) zinc dust, iodine / 1.) benzene, 40 deg, , 2.) benzene, reflux, 2 h

2: 17 g / anhydrous formic acid / 0.5 h / Heating

3: 14 g / sulfur / 5 h / 198 - 200 °C

4: 6 g / aq. KOH / ethanol / 3 h / Heating

6: 1.4 g / methanol / 1 h / Heating

With potassium hydroxide; formic acid; iodine; sulfur; zinc; In methanol; ethanol;

Reference yield:

: 35656-89-4
4-(4-bromophenyl)butanoic acid

: 77389-16-3,77389-20-9
p-bromophenacyl ester α-(7-bromo-3,4-dihydro-1-naphthyl)-propionic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 5 g / orthophosphoric acid, phosphorus pentoxide / 10 h / 165 °C

2: 1.) zinc dust, iodine / 1.) benzene, 40 deg, , 2.) benzene, reflux, 2 h

3: 17 g / anhydrous formic acid / 0.5 h / Heating

4: 14 g / sulfur / 5 h / 198 - 200 °C

5: 6 g / aq. KOH / ethanol / 3 h / Heating

6: 1.8 g / methanol / 1 h / Heating

With phosphorus pentaoxide; potassium hydroxide; formic acid; phosphoric acid; iodine; sulfur; zinc; In methanol; ethanol;