1,3-bis(bromomethyl)-2-methoxymethylbenzene

Base Information

Chemical Name:1,3-bis(bromomethyl)-2-methoxymethylbenzene
CAS No.:131980-50-2
Molecular Formula:C₁₀H₁₂Br₂O
Molecular Weight:308.013
Hs Code.:

Synonyms:

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Chemical Property of 1,3-bis(bromomethyl)-2-methoxymethylbenzene

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Technology Process of 1,3-bis(bromomethyl)-2-methoxymethylbenzene

There total 10 articles about 1,3-bis(bromomethyl)-2-methoxymethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 131980-48-8
2-methoxymethylbenzene-1,3-dimethanol

: 131980-50-2
1,3-bis(bromomethyl)-2-methoxymethylbenzene

Guidance literature:: With phosphorus tribromide; In benzene; for 6h; Ambient temperature;
DOI:10.1071/CH9901783

Reference yield:

: 15120-47-5
2-methyl-1,3-benzenedicarbocylic acid

: 131980-50-2
1,3-bis(bromomethyl)-2-methoxymethylbenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / concd. H₂SO₄ / 24 h / Heating

2: 93 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 0.5 h / Heating; Irradiation

3: 88 percent / methanol / 15 h / Heating

4: 69 percent / LiAlH₄ / tetrahydrofuran / 15 h / Ambient temperature

5: 18 percent / PBr₃ / benzene / 6 h / Ambient temperature

With N-Bromosuccinimide; lithium aluminium tetrahydride; Perbenzoic acid; sulfuric acid; phosphorus tribromide; In tetrahydrofuran; methanol; tetrachloromethane; benzene;
DOI:10.1071/CH9901783

Reference yield:

: 33486-90-7
1,3-dichloro-2-methoxymethylbenzene

: 131980-50-2
1,3-bis(bromomethyl)-2-methoxymethylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 44 percent / various solvent(s) / 30 h / Heating

2: 42 percent / diisobutylaluminium hydride / benzene / 15 h / Ambient temperature

3: 56 percent / NaBH₄ / tetrahydrofuran / 15 h / Ambient temperature

4: 18 percent / PBr₃ / benzene / 6 h / Ambient temperature

With sodium tetrahydroborate; phosphorus tribromide; diisobutylaluminium hydride; In tetrahydrofuran; benzene;
DOI:10.1071/CH9901783