Technology Process of C14H19BrFN3O2
There total 5 articles about C14H19BrFN3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: thionyl chloride / N,N-dimethyl-formamide / dichloromethane
2: triethylamine / dichloromethane
3: piperidine
4: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / tetrahydrofuran / 1 h / 20 °C
With
piperidine; thionyl chloride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine;
N,N-dimethyl-formamide;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium carbonate / 1,4-dioxane; water / 4 h / 20 °C
2: thionyl chloride / N,N-dimethyl-formamide / dichloromethane
3: triethylamine / dichloromethane
4: piperidine
5: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / tetrahydrofuran / 1 h / 20 °C
With
piperidine; thionyl chloride; sodium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine;
N,N-dimethyl-formamide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water;