1,3-diiodo-2,4-diphenylnaphthalene

Base Information

Chemical Name:1,3-diiodo-2,4-diphenylnaphthalene
CAS No.:1370697-61-2
Molecular Formula:C₂₂H₁₄I₂
Molecular Weight:532.162
Hs Code.:

Synonyms:

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Chemical Property of 1,3-diiodo-2,4-diphenylnaphthalene

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Technology Process of 1,3-diiodo-2,4-diphenylnaphthalene

There total 3 articles about 1,3-diiodo-2,4-diphenylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 71-23-8
propan-1-ol

: 1370697-38-3
1-(2-((4-methoxyphenyl)ethynyl)phenyl)-1,3-diphenylprop-2-yn-1-ol

: 1370697-61-2
1,3-diiodo-2,4-diphenylnaphthalene

: 6938-39-2
n-propyl 4-methoxybenzoate

Guidance literature:: With Iodine monochloride; at 23 - 25 ℃; regioselective reaction;
DOI:10.1021/ol300457c

Reference yield:

: 25187-00-2
2-iodobenzophenone

: 1370697-61-2
1,3-diiodo-2,4-diphenylnaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 0.25 h / 23 - 25 °C / Inert atmosphere

1.2: 4 h / 50 °C / Inert atmosphere

2.1: ethylmagnesium bromide / tetrahydrofuran / 0.5 h / 40 °C

2.2: 23 - 25 °C

3.1: Iodine monochloride / 23 - 25 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; ethylmagnesium bromide; Iodine monochloride; triethylamine; In tetrahydrofuran;
DOI:10.1021/ol300457c

Reference yield:

: 1370697-68-9
(2-((4-methoxyphenyl)ethynyl)phenyl) (phenyl)methanone

: 1370697-61-2
1,3-diiodo-2,4-diphenylnaphthalene

: 6938-39-2
n-propyl 4-methoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethylmagnesium bromide / tetrahydrofuran / 0.5 h / 40 °C

1.2: 23 - 25 °C

2.1: Iodine monochloride / 23 - 25 °C

With ethylmagnesium bromide; Iodine monochloride; In tetrahydrofuran;
DOI:10.1021/ol300457c