2--3-diisopropylaminocarbonylpyridine

Base Information

Chemical Name:2--3-diisopropylaminocarbonylpyridine
CAS No.:148760-59-2
Molecular Formula:C₂₆H₄₀N₄O
Molecular Weight:424.63
Hs Code.:

2-<N-Benzyl-N-(3-diethylaminopropyl)amino>-3-diisopropylaminocarbonylpyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2--3-diisopropylaminocarbonylpyridine

Chemical Property:

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Technology Process of 2--3-diisopropylaminocarbonylpyridine

There total 4 articles about 2--3-diisopropylaminocarbonylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 92377-05-4
N-Benzyl-3-diethylaminopropylamine

: 53063-03-9
2-Chloro-3-diisopropylaminocarbonylpyridine

: 148760-59-2
2--3-diisopropylaminocarbonylpyridine

Guidance literature:: With copper; potassium iodide; at 120 ℃; for 24h;
DOI:10.1016/S0040-4020(01)80387-2

Reference yield:

: 49609-84-9
2-Chloronicotinoyl chloride

: 148760-59-2
2--3-diisopropylaminocarbonylpyridine

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 0.5 h / T < 20 deg C

2: 57 percent / KI, Cu-powder / 24 h / 120 °C

With copper; potassium iodide; In dichloromethane;
DOI:10.1016/S0040-4020(01)80387-2

Reference yield:

: 2942-59-8
2-chloronicotinic acid

: 148760-59-2
2--3-diisopropylaminocarbonylpyridine

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / 3 h / Heating

2: CH₂Cl₂ / 0.5 h / T < 20 deg C

3: 57 percent / KI, Cu-powder / 24 h / 120 °C

With thionyl chloride; copper; potassium iodide; In dichloromethane;
DOI:10.1016/S0040-4020(01)80387-2