TlMes₃

Base Information

Chemical Name:TlMes₃
CAS No.:187877-83-4
Molecular Formula:C₂₇H₃₃Tl
Molecular Weight:561.942
Hs Code.:

Synonyms:

Suppliers and Price of TlMes₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of TlMes₃

Chemical Property:

Purity/Quality:

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Technology Process of TlMes₃

There total 1 articles about TlMes₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.1%

: 13453-32-2
thallium (III) chloride

: 2633-66-1
2-mesitylmagnesium bromide

: 187877-83-4
TlMes₃

Guidance literature:: In tetrahydrofuran; byproducts: MgBrCl; cooling (0°C), refluxing (1 h), stirring (18 h, room temp.); evapn., extraction (toluene), filtn., evapn. (vac.), extraction (n-pentane), evapn.; elem. anal.;
DOI:10.1002/zaac.19976230150

Reference yield: 79.0%

: 187877-83-4
TlMes₃

: 13453-32-2
thallium (III) chloride

: [(Mes₂TlCl)(MesTlCl₂)]

Guidance literature:: In toluene; TlCl3 added to toluene soln. of TlMes3 at 0°C; left standing for 12 h; heated under reflux for 1 h; filtered when hot; cooled to 20°C; warmed and cooled again; elem.anal.;
DOI:10.1002/zaac.200600092

Reference yield:

: 187877-83-4
TlMes₃

: 109-63-7
boron trifluoride diethyl etherate

: (TlMes₂)[BF₄]

Guidance literature:: In diethyl ether; byproducts: BMes3, OEt2; 20 °C, under Ar, excess of B-compd. was added dropwise to Et2O soln. of Tl-compd., stirring for 18 h; ppt. was vac. filtered, washed with n-pentane, solid was filtered off, recrystd. from MeCN, elem. anal.;
DOI:10.1002/zaac.200700033