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Ru(2-(phenylazo)pyridine)2Cl2

Base Information Edit
  • Chemical Name:Ru(2-(phenylazo)pyridine)2Cl2
  • CAS No.:74006-30-7
  • Molecular Formula:C22H18Cl2N6Ru
  • Molecular Weight:538.401
  • Hs Code.:
  • Mol file:74006-30-7.mol
Ru(2-(phenylazo)pyridine)2Cl<sub>2</sub>

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Chemical Property of Ru(2-(phenylazo)pyridine)2Cl2 Edit
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Technology Process of Ru(2-(phenylazo)pyridine)2Cl2

There total 14 articles about Ru(2-(phenylazo)pyridine)2Cl2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
2-(phenylazo)pyridine; C94H87Cl3N11O14Ru; With triethylamine; lithium chloride; In ethanol; water; Reflux;
With ammonium hexafluorophosphate; In ethanol; water;
DOI:10.1021/jacs.7b05458
Guidance literature:
In methanol; byproducts: silver chloride; heating (water bath, 40°C, 15 min, Ru compd. /Ag compd. 1/1); filtration, washing (MeOH), drying (vac.), extn. (CH2Cl2, removal AgCl), crystn. (hexane), filtrates and washings concd., pptn. (H2O), drying, chromy. (silica gel, CH2Cl2/CH3CN);
DOI:10.1039/DT9910003249
Guidance literature:
In N,N-dimethyl-formamide; soln. (Ru(bpy)Cl3)n*xH2O in DMF was mixed withazpy and refluxed for 50 min; react. mixt. was filtered and evapd. to dryness, residue was dissolved in CHCl3, filtered and concd., chromy. on alumina with CHCl3 as eluent, recrystn. from CHCl3-ether; elem. anal.;
DOI:10.1021/ic035390f
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