(-)-dibenzacridine (5S,6S)-dihydrodiol

Base Information

Chemical Name:(-)-dibenzacridine (5S,6S)-dihydrodiol
CAS No.:101313-27-3
Molecular Formula:C₂₁H₁₅NO₂
Molecular Weight:313.356
Hs Code.:

(-)-dibenz<c,h>acridine (5S,6S)-dihydrodiol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-dibenzacridine (5S,6S)-dihydrodiol

Chemical Property:

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Technology Process of (-)-dibenzacridine (5S,6S)-dihydrodiol

There total 12 articles about (-)-dibenzacridine (5S,6S)-dihydrodiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 224-53-3
dibenz[c,h]acridine

: 93716-21-3,93716-22-4,101313-26-2,101313-27-3,104420-69-1
cis-5,6-dihydroxy-5,6-dihydrodibenzacridine

Guidance literature:: With pyridine; osmium(VIII) oxide; for 96h;
DOI:10.1021/jo00201a019

Reference yield: 6.0%

: 67977-00-8
4b,5a-dihydrodibenzoxireno acridine

: 93716-21-3
trans-5,6-dihydroxy-5,6-dihydrodibenzacridine

: 93716-21-3,93716-22-4,101313-26-2,101313-27-3,104420-69-1
cis-5,6-dihydroxy-5,6-dihydrodibenzacridine

Guidance literature:: With acetic acid; at 38 - 40 ℃; for 88h;
DOI:10.1021/jo00201a019

Reference yield:

: 90-15-3
α-naphthol

: 93716-21-3,93716-22-4,101313-26-2,101313-27-3,104420-69-1
cis-5,6-dihydroxy-5,6-dihydrodibenzacridine

Guidance literature:: Multi-step reaction with 4 steps

1: 12.9 percent / 0.25 h / 250 °C

2: 10percent Pd/C / 3 h / 330 - 350 °C

3: 10 percent / aq. NaOCl / tetrabutylammonium hydrogen sulfate / CHCl₃ / 5 h / Ambient temperature

4: aq. HOAc / 88 h / 38 - 40 °C

With sodium hypochlorite; acetic acid; palladium on activated charcoal; tetra(n-butyl)ammonium hydrogensulfate; In chloroform;
DOI:10.1021/jo00201a019