glycyl-L-phenylalanyl-L-citrulline p-nitroanilide hydrobromide

Base Information

Chemical Name:glycyl-L-phenylalanyl-L-citrulline p-nitroanilide hydrobromide
CAS No.:83575-51-3
Molecular Formula:BrH*C₂₃H₂₉N₇O₆
Molecular Weight:580.438
Hs Code.:

Synonyms:

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Chemical Property of glycyl-L-phenylalanyl-L-citrulline p-nitroanilide hydrobromide

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Technology Process of glycyl-L-phenylalanyl-L-citrulline p-nitroanilide hydrobromide

There total 4 articles about glycyl-L-phenylalanyl-L-citrulline p-nitroanilide hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83575-37-5
Nα-benzyloxycarbonyl-L-citrulline p-nitroanilide

: 83575-51-3
glycyl-L-phenylalanyl-L-citrulline p-nitroanilide hydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1: HBr in HOAc / acetic acid / 1.5 h / Ambient temperature

2: 1.) N-methylmorpholine, 1-hydroxybenzotriazole, 2.) dicyclohexylcarbodiimide / 2.) DMF, -5 deg C, 45 min., 3.) room temp., 20 h

3: HBr in HOAc / 1.5 h

With 4-methyl-morpholine; hydrogen bromide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In acetic acid;
DOI:10.1016/0040-4020(82)80232-9

Reference yield:

: 83575-50-2
benzyloxycarbonylglycyl-L-phenylalanyl-L-citrulline p-nitroanilide

: 83575-51-3
glycyl-L-phenylalanyl-L-citrulline p-nitroanilide hydrobromide

Guidance literature:: With hydrogen bromide; for 1.5h;
DOI:10.1016/0040-4020(82)80232-9

Reference yield:

: 1170-76-9
Z-Gly-(L)-Phe

: 83575-51-3
glycyl-L-phenylalanyl-L-citrulline p-nitroanilide hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N-methylmorpholine, 1-hydroxybenzotriazole, 2.) dicyclohexylcarbodiimide / 2.) DMF, -5 deg C, 45 min., 3.) room temp., 20 h

2: HBr in HOAc / 1.5 h

With 4-methyl-morpholine; hydrogen bromide; benzotriazol-1-ol; dicyclohexyl-carbodiimide;
DOI:10.1016/0040-4020(82)80232-9