bis(pentachlorophenyl)ketene methyl isopropyl acetal

Base Information

Chemical Name:bis(pentachlorophenyl)ketene methyl isopropyl acetal
CAS No.:107846-84-4
Molecular Formula:C₁₈H₁₀Cl₁₀O₂
Molecular Weight:612.806
Hs Code.:

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Chemical Property of bis(pentachlorophenyl)ketene methyl isopropyl acetal

Chemical Property:

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Technology Process of bis(pentachlorophenyl)ketene methyl isopropyl acetal

There total 6 articles about bis(pentachlorophenyl)ketene methyl isopropyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 431-47-0
trifluoroacetic acid-methyl ester

: 107846-83-3
sodium 1-isopropoxy-2,2-bis(pentachlorophenyl)ethenolate

: 107846-84-4
bis(pentachlorophenyl)ketene methyl isopropyl acetal

Guidance literature:: at -5 ℃;
DOI:10.1021/jo00386a046

Reference yield:

: 112312-91-1
isopropyl decachlorobenzilate

: 107846-84-4
bis(pentachlorophenyl)ketene methyl isopropyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: PBr₃ / bis-(2-methoxy-ethyl) ether / Heating

2: 1) NaH / 1) THF, 30 deg C, 1 h, 2) RT, 1 h

With phosphorus tribromide; sodium hydride; In diethylene glycol dimethyl ether;
DOI:10.1021/jo00042a021

Reference yield:

: 107846-82-2
isopropyl bis-(pentachlorophenyl)acetate

: 107846-84-4
bis(pentachlorophenyl)ketene methyl isopropyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / tetrahydrofuran

2: 70 percent / -5 °C

With sodium hydride; In tetrahydrofuran;
DOI:10.1021/jo00386a046