C₂₈H₃₆N₂O₅

Base Information

Chemical Name:C₂₈H₃₆N₂O₅
CAS No.:1422740-23-5
Molecular Formula:C₂₈H₃₆N₂O₅
Molecular Weight:480.604
Hs Code.:

C<sub>28</sub>H<sub>36</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₂₈H₃₆N₂O₅

Chemical Property:

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Technology Process of C₂₈H₃₆N₂O₅

There total 14 articles about C₂₈H₃₆N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 773837-37-9
sodium cyanide

: C₃₄H₄₃NO₈S

: 1422740-23-5
C₂₈H₃₆N₂O₅

Guidance literature:: With sodium hydrogencarbonate; In dimethyl sulfoxide; at 60 ℃; for 8h;
DOI:10.3762/bjoc.8.210

Reference yield:

: 126587-35-7
methyl (4S)-4-[(tert-butoxy)carbonylamino]-5-hydroxypentanoate

: 1422740-23-5
C₂₈H₃₆N₂O₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: boron trifluoride diethyl etherate; 2,2-dimethoxy-propane / 0.5 h / 20 °C

2.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; diisopropylamine / tetrahydrofuran / 0.5 h / -78 °C

2.2: 3 h / -78 °C

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / -40 °C

4.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / 0 °C

5.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tert-butyl alcohol / 24 h / 20 °C

6.1: triethylamine / dichloromethane / 24 h / 0 - 20 °C

7.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C

7.2: 72 h / 20 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 0 - 20 °C

9.1: pyridine / 0.67 h / 0 °C

10.1: sodium hydrogencarbonate / dimethyl sulfoxide / 8 h / 60 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; osmium(VIII) oxide; n-butyllithium; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; 4-methylmorpholine N-oxide; triethylamine; diisopropylamine; 3-chloro-benzenecarboperoxoic acid; 2,2-dimethoxy-propane; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; toluene; mineral oil; tert-butyl alcohol; 3.1: |Wittig-Horner Reaction;
DOI:10.3762/bjoc.8.210

Reference yield:

: 96014-55-0
Methyl (4S)-4-(N-(tert-Butoxycarbonyl)amino)-5-((tert-butyldimethylsilyl)oxy)pentanoate

: 1422740-23-5
C₂₈H₃₆N₂O₅

Guidance literature:: Multi-step reaction with 11 steps

1.1: toluene-4-sulfonic acid / methanol / 3 h / 20 °C

2.1: boron trifluoride diethyl etherate; 2,2-dimethoxy-propane / 0.5 h / 20 °C

3.1: N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; diisopropylamine / tetrahydrofuran / 0.5 h / -78 °C

3.2: 3 h / -78 °C

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / -40 °C

5.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / 0 °C

6.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tert-butyl alcohol / 24 h / 20 °C

7.1: triethylamine / dichloromethane / 24 h / 0 - 20 °C

8.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C

8.2: 72 h / 20 °C

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 0 - 20 °C

10.1: pyridine / 0.67 h / 0 °C

11.1: sodium hydrogencarbonate / dimethyl sulfoxide / 8 h / 60 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; osmium(VIII) oxide; n-butyllithium; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; triethylamine; diisopropylamine; 3-chloro-benzenecarboperoxoic acid; 2,2-dimethoxy-propane; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; toluene; mineral oil; tert-butyl alcohol; 4.1: |Wittig-Horner Reaction;
DOI:10.3762/bjoc.8.210