C₂₄H₁₉F₂NO₄

Base Information

Chemical Name:C₂₄H₁₉F₂NO₄
CAS No.:1417404-53-5
Molecular Formula:C₂₄H₁₉F₂NO₄
Molecular Weight:423.416
Hs Code.:

C<sub>24</sub>H<sub>19</sub>F<sub>2</sub>NO<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₁₉F₂NO₄

Chemical Property:

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Technology Process of C₂₄H₁₉F₂NO₄

There total 15 articles about C₂₄H₁₉F₂NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₁₂Cl₂O₃

: 1417404-53-5
C₂₄H₁₉F₂NO₄

Guidance literature:: Multi-step reaction with 7 steps

1: aluminum (III) chloride / dichloromethane / 0.33 h / 0 °C

2: thionyl chloride / dichloromethane / 1 h / Reflux

3: dichloromethane / 0 - 20 °C

4: palladium diacetate; XPhos; potassium tert-butylate / toluene; tert-butyl alcohol / 2 h / 100 °C / Inert atmosphere

5: hydrogenchloride; water / 6 h / Reflux

6: thionyl chloride / tetrahydrofuran / 1 h / Reflux

7: dichloromethane / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; aluminum (III) chloride; thionyl chloride; potassium tert-butylate; water; palladium diacetate; XPhos; In tetrahydrofuran; dichloromethane; toluene; tert-butyl alcohol; 1: |Friedel-Crafts Acylation / 4: |Buchwald-Hartwig Coupling;
DOI:10.1021/jm301539x

Reference yield:

: C₁₆H₁₀Cl₂O₂

: 1417404-53-5
C₂₄H₁₉F₂NO₄

Guidance literature:: Multi-step reaction with 5 steps

1: dichloromethane / 0 - 20 °C

2: palladium diacetate; XPhos; potassium tert-butylate / toluene; tert-butyl alcohol / 2 h / 100 °C / Inert atmosphere

3: hydrogenchloride; water / 6 h / Reflux

4: thionyl chloride / tetrahydrofuran / 1 h / Reflux

5: dichloromethane / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; thionyl chloride; potassium tert-butylate; water; palladium diacetate; XPhos; In tetrahydrofuran; dichloromethane; toluene; tert-butyl alcohol; 2: |Buchwald-Hartwig Coupling;
DOI:10.1021/jm301539x

Reference yield:

: 1943-88-0
2,4-dicyanotoluene

: 1417404-53-5
C₂₄H₁₉F₂NO₄

Guidance literature:: Multi-step reaction with 12 steps

1.1: water; sodium hydroxide / diethylene glycol / 120 h / Reflux

2.1: sulfuric acid / 6 h / Reflux

3.1: n-butyllithium; diisopropylamine / hexane; tetrahydrofuran / 1 h / -78 - 0 °C

3.2: -78 - 0 °C

4.1: potassium hydroxide / methanol / 6 h / Reflux

5.1: thionyl chloride / dichloromethane / Reflux

6.1: aluminum (III) chloride / dichloromethane / 0.33 h / 0 °C

7.1: thionyl chloride / dichloromethane / 1 h / Reflux

8.1: dichloromethane / 0 - 20 °C

9.1: palladium diacetate; XPhos; potassium tert-butylate / toluene; tert-butyl alcohol / 2 h / 100 °C / Inert atmosphere

10.1: hydrogenchloride; water / 6 h / Reflux

11.1: thionyl chloride / tetrahydrofuran / 1 h / Reflux

12.1: dichloromethane / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; aluminum (III) chloride; n-butyllithium; thionyl chloride; sulfuric acid; potassium tert-butylate; water; palladium diacetate; diisopropylamine; potassium hydroxide; sodium hydroxide; XPhos; In tetrahydrofuran; methanol; hexane; dichloromethane; toluene; tert-butyl alcohol; diethylene glycol; 6.1: |Friedel-Crafts Acylation / 9.1: |Buchwald-Hartwig Coupling;
DOI:10.1021/jm301539x