[Co(II)(α-benzyldioxime-H)2(pyridine)2]

Base Information

Chemical Name:[Co(II)(α-benzyldioxime-H)2(pyridine)2]
CAS No.:42957-80-2
Molecular Formula:C₃₈H₃₂CoN₆O₄
Molecular Weight:695.703
Hs Code.:

Synonyms:

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Chemical Property of [Co(II)(α-benzyldioxime-H)2(pyridine)2]

Chemical Property:

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Technology Process of [Co(II)(α-benzyldioxime-H)2(pyridine)2]

There total 1 articles about [Co(II)(α-benzyldioxime-H)2(pyridine)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 110-86-1
pyridine

: cobalt(II) chloride hexahydrate

: 23873-81-6
benzildioxime

: 42957-80-2
[Co(II)(α-benzyldioxime-H)2(pyridine)2]

Guidance literature:: In ethanol; under Ar; CoCl2*6H2O (27.3 mmol) and pyridine (130 mmol) were dissolved in ethanol; stirring for 4 min; a ligand (52 mmol) and ethanol were added; the soln. was stirred for 11 h and left overnight; the mixt. was filtered under Ar; the solid was washed with ethanol and dried in vac.;
DOI:10.1039/c2dt12513g

Reference yield: 82.0%

: 42957-80-2
[Co(II)(α-benzyldioxime-H)2(pyridine)2]

: 109-63-7
trifluoroborane diethyl ether

: 75-05-8,26809-02-9
acetonitrile

: 130247-28-8
(difluoroboryl)diphenylglyoximatocobalt(II) bis(acetonitrile)

Guidance literature:: With hexamethyldisiloxane; In diethyl ether; acetonitrile; under Ar; Co-contg. compd. (35.8 mmol) and hexamethyldisiloxane were dissolved/suspended in diethyl ether-acetonitrile 1:1 mixt.; stirring for 5min; dropwise addn. (for 5 min) of B-contg. compd. (180 mmol); stirring for 5 min; the ppt. was filtered and washed with Et2O-CH3CN, Et2O-CH3CN-hexamethyldisiloxane and dried in vac.;
DOI:10.1039/c2dt12513g

Reference yield:

: 42957-80-2
[Co(II)(α-benzyldioxime-H)2(pyridine)2]

: 1376083-66-7
Co(II)(α-benzyldioxime-2H)2(S2-Nx)(BF)2

Guidance literature:: Multi-step reaction with 3 steps

1: hexamethyldisiloxane / acetonitrile; diethyl ether

2: triethylamine; hexamethyldisiloxane / nitromethane

3: triethylamine / dichloromethane

With hexamethyldisiloxane; triethylamine; In diethyl ether; nitromethane; dichloromethane; acetonitrile;
DOI:10.1039/c2dt12513g