Technology Process of C27H26O4S
There total 4 articles about C27H26O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
ethanol; water; toluene;
at 80 ℃;
Inert atmosphere;
DOI:10.1021/co200090p
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; triethylamine / 50 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; cyclohexane / 1.5 h / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
3.1: iodine / dichloromethane / 0.17 h / 20 °C
4.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; water; toluene / 80 °C / Inert atmosphere
With
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; trans-bis(triphenylphosphine)palladium dichloride; iodine; potassium carbonate; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; cyclohexane; water; toluene;
1.1: Sonogashira reaction / 4.1: Suzuki-Miyaura coupling;
DOI:10.1021/co200090p
- Guidance literature:
-
Multi-step reaction with 2 steps
1: iodine / dichloromethane / 0.17 h / 20 °C
2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol; water; toluene / 80 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); iodine; potassium carbonate;
In
ethanol; dichloromethane; water; toluene;
2: Suzuki-Miyaura coupling;
DOI:10.1021/co200090p
