C₃₈H₂₇F₃N₄

Base Information

Chemical Name:C₃₈H₂₇F₃N₄
CAS No.:1629023-89-7
Molecular Formula:C₃₈H₂₇F₃N₄
Molecular Weight:596.654
Hs Code.:

C<sub>38</sub>H<sub>27</sub>F<sub>3</sub>N<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₈H₂₇F₃N₄

Chemical Property:

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Technology Process of C₃₈H₂₇F₃N₄

There total 11 articles about C₃₈H₂₇F₃N₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-05-4,9003-20-7
vinyl acetate

: 1629023-85-3
C₃₆H₂₄BrF₃N₄

: 1629023-89-7
C₃₈H₂₇F₃N₄

: 1629600-76-5
C₄₀H₂₉F₃N₄O₂

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; at 130 ℃; for 0.5h; Overall yield = 73 %; Microwave irradiation;
DOI:10.1016/j.bmcl.2014.05.082

Reference yield:

: 1160502-31-7
4-iodo-3-(trifluoromethyl)-1-tritylpyrazolo[5,4-b]pyridine

: 1629023-89-7
C₃₈H₂₇F₃N₄

: 1629600-76-5
C₄₀H₂₉F₃N₄O₂

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; 1,4-di(diphenylphosphino)-butane; tert-butylamine; propyl cyanide / water / 16 h / 120 °C

2: bis(tri-t-butylphosphine)palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine / 1,4-dioxane / 0.5 h / 130 °C / Microwave irradiation

With propyl cyanide; bis(tri-t-butylphosphine)palladium⁽⁰⁾; palladium diacetate; tert-butylamine; N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane; In 1,4-dioxane; water; 1: |Suzuki Coupling / 2: |Heck Reaction;
DOI:10.1016/j.bmcl.2014.05.082

Reference yield:

: 153034-82-3
[(fluoro-2-iodo-4)pyrid-3-yl]-carboxaldehyde

: 1629023-89-7
C₃₈H₂₇F₃N₄

: 1629600-76-5
C₄₀H₂₉F₃N₄O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / -10 - 0 °C

2.1: manganese(IV) oxide / toluene / 3 h / Reflux

3.1: hydrazine hydrate / 1,4-dioxane / 0.25 h / 50 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C

4.2: 2 h / 20 °C

5.1: palladium diacetate; 1,4-di(diphenylphosphino)-butane; tert-butylamine; propyl cyanide / water / 16 h / 120 °C

6.1: bis(tri-t-butylphosphine)palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine / 1,4-dioxane / 0.5 h / 130 °C / Microwave irradiation

With manganese(IV) oxide; propyl cyanide; bis(tri-t-butylphosphine)palladium⁽⁰⁾; tetrabutyl ammonium fluoride; palladium diacetate; sodium hydride; hydrazine hydrate; tert-butylamine; N-ethyl-N,N-diisopropylamine; 1,4-di(diphenylphosphino)-butane; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; toluene; 5.1: |Suzuki Coupling / 6.1: |Heck Reaction;
DOI:10.1016/j.bmcl.2014.05.082