acide methoxy-3 dimethyl-2,2 methylene-6 cyclohexanecarboxylique (1RS,3RS)

Base Information

Chemical Name:acide methoxy-3 dimethyl-2,2 methylene-6 cyclohexanecarboxylique (1RS,3RS)
CAS No.:79693-51-9
Molecular Formula:C₁₁H₁₈O₃
Molecular Weight:198.262
Hs Code.:

Synonyms:

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Chemical Property of acide methoxy-3 dimethyl-2,2 methylene-6 cyclohexanecarboxylique (1RS,3RS)

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Technology Process of acide methoxy-3 dimethyl-2,2 methylene-6 cyclohexanecarboxylique (1RS,3RS)

There total 6 articles about acide methoxy-3 dimethyl-2,2 methylene-6 cyclohexanecarboxylique (1RS,3RS) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4454-05-1
2-methoxy-3,4-dihydro-2H-pyran

: 79693-51-9,79733-17-8
acide methoxy-3 dimethyl-2,2 methylene-6 cyclohexanecarboxylique (1RS,3RS)

Guidance literature:: Multi-step reaction with 6 steps

1: 55 percent / boron trifluoride-methanol complex / methanol / 4 h / Heating

2: 61 percent / boron trifluoride etherate / Ambient temperature

3: 95 percent / sodium acetate / acetic acid; H₂O / 4 h / Heating

4: 92 percent / NaBH₄ / methanol; H₂O / 1 h / Ambient temperature

5: 73 percent / triphenylphosphine / CCl₄ / 4 h / Heating

6: 1.) Mg, iodine / 1.) THF, -17 deg C, 2.) -100 deg C, 35 min

With sodium tetrahydroborate; boron trifluoride diethyl etherate; iodine; sodium acetate; boron trifluoride methanol complex; magnesium; triphenylphosphine; In methanol; tetrachloromethane; water; acetic acid;

Reference yield:

: 4454-02-8
1,1,5,5-tetramethoxy-pentane

: 79693-51-9,79733-17-8
acide methoxy-3 dimethyl-2,2 methylene-6 cyclohexanecarboxylique (1RS,3RS)

Guidance literature:: Multi-step reaction with 5 steps

1: 61 percent / boron trifluoride etherate / Ambient temperature

2: 95 percent / sodium acetate / acetic acid; H₂O / 4 h / Heating

3: 92 percent / NaBH₄ / methanol; H₂O / 1 h / Ambient temperature

4: 73 percent / triphenylphosphine / CCl₄ / 4 h / Heating

5: 1.) Mg, iodine / 1.) THF, -17 deg C, 2.) -100 deg C, 35 min

With sodium tetrahydroborate; boron trifluoride diethyl etherate; iodine; sodium acetate; magnesium; triphenylphosphine; In methanol; tetrachloromethane; water; acetic acid;

Reference yield:

: 73739-62-5
formyl-1 methoxy-4 dimethyl-3,3 cyclohexene-1

: 79693-51-9,79733-17-8
acide methoxy-3 dimethyl-2,2 methylene-6 cyclohexanecarboxylique (1RS,3RS)

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / NaBH₄ / methanol; H₂O / 1 h / Ambient temperature

2: 73 percent / triphenylphosphine / CCl₄ / 4 h / Heating

3: 1.) Mg, iodine / 1.) THF, -17 deg C, 2.) -100 deg C, 35 min

With sodium tetrahydroborate; iodine; magnesium; triphenylphosphine; In methanol; tetrachloromethane; water;