Technology Process of (2-Carboxymethoxy-5-methoxy-phenyl)-acetic acid
There total 4 articles about (2-Carboxymethoxy-5-methoxy-phenyl)-acetic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride; hydrogen iodide; acetic acid; tin(ll) chloride;
for 3h;
Heating;
DOI:10.1002/bscb.19800890607
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 80 percent / potassium carbonate, potassium iodide / 4 h / Heating
2: 1.) potassium metabisulfite / 1.) 50 deg C, water 2.) water, ether, 5 deg C, 6 h
3: stannous chloride dihydrate, cc. hydrogen chloride, acetic acid, hydrogen iodide / 3 h / Heating
With
hydrogenchloride; potassium disulphite; hydrogen iodide; potassium carbonate; acetic acid; potassium iodide; tin(ll) chloride;
DOI:10.1002/bscb.19800890607
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) potassium metabisulfite / 1.) 50 deg C, water 2.) water, ether, 5 deg C, 6 h
2: stannous chloride dihydrate, cc. hydrogen chloride, acetic acid, hydrogen iodide / 3 h / Heating
With
hydrogenchloride; potassium disulphite; hydrogen iodide; acetic acid; tin(ll) chloride;
DOI:10.1002/bscb.19800890607