Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-10,13-dimethyl-7-(2-1,4,7,10-tetraoxa-13-aza-cyclopentadec-13-yl-acetoxy)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Base Information

• Chemical Name: Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-10,13-dimethyl-7-(2-1,4,7,10-tetraoxa-13-aza-cyclopentadec-13-yl-acetoxy)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester
• CAS No.: 907205-62-3
• Molecular Formula: C₆₀H₇₅NO₁₀
• Molecular Weight: 970.256

Synonyms:

Chemical Property of Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-10,13-dimethyl-7-(2-1,4,7,10-tetraoxa-13-aza-cyclopentadec-13-yl-acetoxy)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-10,13-dimethyl-7-(2-1,4,7,10-tetraoxa-13-aza-cyclopentadec-13-yl-acetoxy)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

There total 5 articles about Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-10,13-dimethyl-7-(2-1,4,7,10-tetraoxa-13-aza-cyclopentadec-13-yl-acetoxy)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl 3α,7α-dihydroxy-5β-cholan-24-oate (111992-94-0) → Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-10,13-dimethyl-7-(2-1,4,7,10-tetraoxa-13-aza-cyclopentadec-13-yl-acetoxy)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester (907205-62-3)

Guidance literature:

Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂

2: tetrabutylammonium iodide; calcium hydride / toluene / Heating

3: sodium carbonate / acetonitrile / Heating

With dmap; calcium hydride; tetra-(n-butyl)ammonium iodide; sodium carbonate; dicyclohexyl-carbodiimide; In dichloromethane; toluene; acetonitrile;

DOI:10.1021/ol061082k

Reference yield:

Pyrene-1-carboxylic acid (3R,5R,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester (907205-58-7) → Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-10,13-dimethyl-7-(2-1,4,7,10-tetraoxa-13-aza-cyclopentadec-13-yl-acetoxy)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester (907205-62-3)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrabutylammonium iodide; calcium hydride / toluene / Heating

2: sodium carbonate / acetonitrile / Heating

With calcium hydride; tetra-(n-butyl)ammonium iodide; sodium carbonate; In toluene; acetonitrile;

DOI:10.1021/ol061082k

Reference yield:

Pyrene-1-carboxylic acid (19694-02-1) → Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-10,13-dimethyl-7-(2-1,4,7,10-tetraoxa-13-aza-cyclopentadec-13-yl-acetoxy)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester (907205-62-3)

Guidance literature:

Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂

2: tetrabutylammonium iodide; calcium hydride / toluene / Heating

3: sodium carbonate / acetonitrile / Heating

With dmap; calcium hydride; tetra-(n-butyl)ammonium iodide; sodium carbonate; dicyclohexyl-carbodiimide; In dichloromethane; toluene; acetonitrile;

DOI:10.1021/ol061082k

upstream raw materials:

Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-(2-chloro-acetoxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

1,4,7,10-tetraoxa-15-azacyclopentadecane

benzyl 3α,7α-dihydroxy-5β-cholan-24-oate

Pyrene-1-carboxylic acid (3R,5R,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 907205-62-3 Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-10,13-dimethyl-7-(2-1,4,7,10-tetraoxa-13-aza-cyclopentadec-13-yl-acetoxy)-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send