Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-(2-chloro-acetoxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Base Information

Chemical Name:Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-(2-chloro-acetoxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester
CAS No.:907205-60-1
Molecular Formula:C₅₀H₅₅ClO₆
Molecular Weight:787.436
Hs Code.:

Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-(2-chloro-acetoxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

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Chemical Property of Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-(2-chloro-acetoxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Chemical Property:

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Technology Process of Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-(2-chloro-acetoxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

There total 5 articles about Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-(2-chloro-acetoxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 111992-94-0
benzyl 3α,7α-dihydroxy-5β-cholan-24-oate

: 907205-60-1
Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-(2-chloro-acetoxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂

2: tetrabutylammonium iodide; calcium hydride / toluene / Heating

With dmap; calcium hydride; tetra-(n-butyl)ammonium iodide; dicyclohexyl-carbodiimide; In dichloromethane; toluene;
DOI:10.1021/ol061082k

Reference yield:

: 19694-02-1
Pyrene-1-carboxylic acid

: 907205-60-1
Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-(2-chloro-acetoxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂

2: tetrabutylammonium iodide; calcium hydride / toluene / Heating

With dmap; calcium hydride; tetra-(n-butyl)ammonium iodide; dicyclohexyl-carbodiimide; In dichloromethane; toluene;
DOI:10.1021/ol061082k

Reference yield:

: 474-25-9
chenodeoxycholic acid

: 907205-60-1
Pyrene-1-carboxylic acid (3R,5S,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-(2-chloro-acetoxy)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dimethylformamide / 55 °C

2: dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂

3: tetrabutylammonium iodide; calcium hydride / toluene / Heating

With dmap; calcium hydride; tetra-(n-butyl)ammonium iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol061082k