Pyrene-1-carboxylic acid (3R,5R,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Base Information

Chemical Name:Pyrene-1-carboxylic acid (3R,5R,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester
CAS No.:907205-58-7
Molecular Formula:C₄₈H₅₄O₅
Molecular Weight:710.954
Hs Code.:

Pyrene-1-carboxylic acid (3R,5R,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

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Chemical Property of Pyrene-1-carboxylic acid (3R,5R,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

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Technology Process of Pyrene-1-carboxylic acid (3R,5R,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

There total 3 articles about Pyrene-1-carboxylic acid (3R,5R,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 474-25-9
chenodeoxycholic acid

: 907205-58-7
Pyrene-1-carboxylic acid (3R,5R,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dimethylformamide / 55 °C

2: dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂

With dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol061082k

Reference yield:

: 100-39-0
benzyl bromide

: 907205-58-7
Pyrene-1-carboxylic acid (3R,5R,7R,8R,9S,10S,13R,14S,17R)-17-((R)-3-benzyloxycarbonyl-1-methyl-propyl)-7-hydroxy-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dimethylformamide / 55 °C

2: dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂

With dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol061082k