Technology Process of 2,5,8,11,14-Pentaoxahexadecane, 16-chloro-1-phenyl-
There total 7 articles about 2,5,8,11,14-Pentaoxahexadecane, 16-chloro-1-phenyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; thionyl chloride;
In
benzene;
for 2h;
Heating;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 53 percent / sodium hydride / tetrahydrofuran / 24 h / Heating
2: 95 percent / hydrogen / 10percent palladium-charcoal / methanol / 1.5 h / 60 °C / 75006 Torr
3: 70 percent / aq. 50percent sodium hydroxide / 24 h / 100 °C
4: 93 percent / thionyl chloride, pyridine / benzene / 2 h / Heating
With
pyridine; sodium hydroxide; thionyl chloride; hydrogen; sodium hydride;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 95 percent / hydrogen / 10percent palladium-charcoal / methanol / 1.5 h / 60 °C / 75006 Torr
2: 70 percent / aq. 50percent sodium hydroxide / 24 h / 100 °C
3: 93 percent / thionyl chloride, pyridine / benzene / 2 h / Heating
With
pyridine; sodium hydroxide; thionyl chloride; hydrogen;
palladium on activated charcoal;
In
methanol; benzene;
![2-(2-{2-[2-(2-benzyloxyethoxy)ethoxy]ethoxy}ethoxy)ethanol](/Databaselist/images/loading.webp)
