1-(triphenylmethyloxy)-26-(phenylmethyloxy)-3,6,9,12,15,18,21,24-octaoxahexaeicosane

Base Information

Chemical Name:1-(triphenylmethyloxy)-26-(phenylmethyloxy)-3,6,9,12,15,18,21,24-octaoxahexaeicosane
CAS No.:868594-47-2
Molecular Formula:C₄₄H₅₈O₁₀
Molecular Weight:746.939
Hs Code.:

Synonyms:1-(triphenylmethyloxy)-26-(phenylmethyloxy)-3,6,9,12,15,18,21,24-octaoxahexaeicosane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(triphenylmethyloxy)-26-(phenylmethyloxy)-3,6,9,12,15,18,21,24-octaoxahexaeicosane

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 1-(triphenylmethyloxy)-26-(phenylmethyloxy)-3,6,9,12,15,18,21,24-octaoxahexaeicosane

There total 6 articles about 1-(triphenylmethyloxy)-26-(phenylmethyloxy)-3,6,9,12,15,18,21,24-octaoxahexaeicosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 24342-68-5,1201808-31-2
1-phenyl-2,5,8,11,14,17-hexaoxanonadecan-19-ol

: 146462-59-1
1-(methylsulfonyl)-10-(triphenylcarbinyl)-1,4,7,10-tetraoxadecane

: 868594-47-2
1-(triphenylmethyloxy)-26-(phenylmethyloxy)-3,6,9,12,15,18,21,24-octaoxahexaeicosane

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 96h;
DOI:10.1002/ejoc.200701188

Reference yield:

: 57671-28-0,1201808-31-2
2-(2-{2-[2-(2-benzyloxyethoxy)ethoxy]ethoxy}ethoxy)ethanol

: 868594-47-2
1-(triphenylmethyloxy)-26-(phenylmethyloxy)-3,6,9,12,15,18,21,24-octaoxahexaeicosane

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / SOCl₂ / 18 h / 80 °C

2: 1.) K, 2.) Br₂ / 1.) THF, 15 min, 2.) THF, 24 h, reflux

With thionyl chloride; bromine;

Reference yield:

: 4792-15-8
Pentaethylene glycol

: 868594-47-2
1-(triphenylmethyloxy)-26-(phenylmethyloxy)-3,6,9,12,15,18,21,24-octaoxahexaeicosane

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / 50percent NaOH / H₂O / 24 h / Heating

2: 86 percent / SOCl₂ / 18 h / 80 °C

3: 1.) K, 2.) Br₂ / 1.) THF, 15 min, 2.) THF, 24 h, reflux

With sodium hydroxide; thionyl chloride; bromine; In water;