{(η5-C5H5)I2Rh(μ-Ph2PPy)Rh(CO)I3}

Base Information

Chemical Name:{(η5-C5H5)I2Rh(μ-Ph2PPy)Rh(CO)I3}
CAS No.:119326-28-2
Molecular Formula:CO*C₅H₅*C₁₇H₁₄NP*5I*2Rh
Molecular Weight:1196.72
Hs Code.:

Synonyms:

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Chemical Property of {(η5-C5H5)I2Rh(μ-Ph2PPy)Rh(CO)I3}

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Technology Process of {(η5-C5H5)I2Rh(μ-Ph2PPy)Rh(CO)I3}

There total 4 articles about {(η5-C5H5)I2Rh(μ-Ph2PPy)Rh(CO)I3} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 119326-23-7
{(η5-C5H5)Rh(μ-CO)(μ-Ph2PPy)Rh(CO)Cl}

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 119326-28-2
{(η5-C5H5)I2Rh(μ-Ph2PPy)Rh(CO)I3}

Guidance literature:: In dichloromethane; soln. of iodine added to stirred soln. of complex; filtered, concd., Et2O added, slowly evapd.;

Reference yield: 60.0%

: 119326-23-7
{(η5-C5H5)Rh(μ-CO)(μ-Ph2PPy)Rh(CO)Cl}

: 75-11-6
diiodomethane

: 119326-28-2
{(η5-C5H5)I2Rh(μ-Ph2PPy)Rh(CO)I3}

: 119326-27-1
{(η5-C5H5)(μ-I)Rh(μ-Ph2PPy)Rh(CO)I2}

Guidance literature:: In dichloromethane; soln. of complex treated with CH2I2, stirred for 24 h; filtered, evapd., residue dissolved in CH2Cl2, transfered onto a neutral alumina column, (diethyl ether-CH2Cl2 1:1), green fraction slowly evapd., ppt. collected.;

Reference yield: 25.0%

: 119326-23-7
{(η5-C5H5)Rh(μ-CO)(μ-Ph2PPy)Rh(CO)Cl}

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 119326-28-2
{(η5-C5H5)I2Rh(μ-Ph2PPy)Rh(CO)I3}

: 119326-27-1
{(η5-C5H5)(μ-I)Rh(μ-Ph2PPy)Rh(CO)I2}

Guidance literature:: In diethyl ether; soln. of I2 added dropwise to soln. of complex (N2); filtered, extd. with benzene, heptane added, crystals collected; elem. anal.;