C₇₁H₇₄BrNO₁₂SSi

Base Information

Chemical Name:C₇₁H₇₄BrNO₁₂SSi
CAS No.:1314746-26-3
Molecular Formula:C₇₁H₇₄BrNO₁₂SSi
Molecular Weight:1273.42
Hs Code.:

C<sub>71</sub>H<sub>74</sub>BrNO<sub>12</sub>SSi

Synonyms:

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Chemical Property of C₇₁H₇₄BrNO₁₂SSi

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Technology Process of C₇₁H₇₄BrNO₁₂SSi

There total 7 articles about C₇₁H₇₄BrNO₁₂SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1314746-25-2
C₆₉H₇₀BrN₃O₁₁SSi

: 507-09-5
tiolacetic acid

: 1314746-26-3
C₇₁H₇₄BrNO₁₂SSi

Guidance literature:: With pyridine; In chloroform;
DOI:10.1038/nchem.1073

Reference yield:

: 1314746-19-4
C₂₂H₄₁N₃O₄SSi₃

: 1314746-26-3
C₇₁H₇₄BrNO₁₂SSi

Guidance literature:: Multi-step reaction with 7 steps

1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2 h

2: dmap; triethylamine / dichloromethane

3: sodium hydride / N,N-dimethyl-formamide

4: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 4 h / -78 - -20 °C

5: copper(II) bis(trifluoromethanesulfonate)

6: zinc(II) iodide / dichloromethane / 3 h

7: pyridine / chloroform

With pyridine; dmap; N-iodo-succinimide; trifluorormethanesulfonic acid; trimethylsilyl trifluoromethanesulfonate; copper(II) bis(trifluoromethanesulfonate); sodium hydride; triethylamine; zinc(II) iodide; In dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1038/nchem.1073

Reference yield:

: 1314746-20-7
p-methylphenyl 2-azido-2-deoxy-4-O-(2-naphthylmethyl)-1-thio-D-glucopyranoside ⁽⁴⁾

: 1314746-26-3
C₇₁H₇₄BrNO₁₂SSi

Guidance literature:: Multi-step reaction with 6 steps

1: dmap; triethylamine / dichloromethane

2: sodium hydride / N,N-dimethyl-formamide

3: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 4 h / -78 - -20 °C

4: copper(II) bis(trifluoromethanesulfonate)

5: zinc(II) iodide / dichloromethane / 3 h

6: pyridine / chloroform

With pyridine; dmap; N-iodo-succinimide; trifluorormethanesulfonic acid; copper(II) bis(trifluoromethanesulfonate); sodium hydride; triethylamine; zinc(II) iodide; In dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1038/nchem.1073