<3',5'-2H2>-L-tyrosine benzyl ester

Base Information

• Chemical Name: <3',5'-2H2>-L-tyrosine benzyl ester
• CAS No.: 159753-88-5
• Molecular Formula: C₁₆H₁₇NO₃
• Molecular Weight: 273.3
• Mol file: 159753-88-5.mol

Synonyms:

Chemical Property of <3',5'-2H2>-L-tyrosine benzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of <3',5'-2H2>-L-tyrosine benzyl ester

There total 2 articles about <3',5'-2H2>-L-tyrosine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

L-3,5-2H2-tyrosine (30811-19-9) + benzyl alcohol (100-51-6,185532-71-2) → <3',5'-2H2>-L-tyrosine benzyl ester (159753-88-5)

Guidance literature:

With toluene-4-sulfonic acid; at 100 ℃;

DOI:10.1002/jlcr.2580340905

Reference yield:

L-tyrosine (60-18-4,18875-48-4,25619-78-7,30704-25-7) → <3',5'-2H2>-L-tyrosine benzyl ester (159753-88-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 5.4 g / 6N DCl/D₂O / 6 h / Heating

2: 60 percent / p-toluenesulfonic acid / 100 °C

With diclazuril; water-d2; toluene-4-sulfonic acid;

DOI:10.1002/jlcr.2580340905

Reference yield:

<3',5'-2H2>-L-tyrosine benzyl ester (159753-88-5) → <3',5'-2H2>-phenylalanine

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / acetone / Heating

2: H₂ / 10percent Pd/C / ethanol / 24 h / 3800 Torr

With hydrogen; potassium carbonate; palladium on activated charcoal; In ethanol; acetone;

DOI:10.1002/jlcr.2580340905

upstream raw materials:

L-3,5-²H₂-tyrosine

benzyl alcohol

L-tyrosine