AKOS BBS-00006126

Base Information

• Chemical Name: AKOS BBS-00006126
• CAS No.: 1234351-88-2
• Molecular Formula: C₁₆H₁₂O₄
• Molecular Weight: 268.269
• Mol file: 1234351-88-2.mol

Synonyms:

Chemical Property of AKOS BBS-00006126

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

(2Z)-6-Hydroxy-2-(3-methoxybenzylidene)-1-benzofuran-3(2H)-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of AKOS BBS-00006126

There total 1 articles about AKOS BBS-00006126 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

6-hydroxybenzofuran-3-one (6272-26-0) + 3-methoxy-benzaldehyde (591-31-1) → (2Z)-6-hydroxy-2-(3-methoxybenzylidene)-1-benzofuran-3(2H)-one (1234351-88-2)

Guidance literature:

With hydrogenchloride; In ethanol; water; at 60 - 70 ℃;

DOI:10.1016/j.bmcl.2011.05.117

Reference yield:

(2Z)-6-hydroxy-2-(3-methoxybenzylidene)-1-benzofuran-3(2H)-one (1234351-88-2) + 1-(3-chloropropyl)pyrrolidine hydrochloride (57616-69-0) → (Z)-2-(3-methoxybenzylidene)-6-(3-(pyrrolidin-1-yl)propoxy)benzofuran-3(2H)-one hydrochloride

Guidance literature:

(2Z)-6-hydroxy-2-(3-methoxybenzylidene)-1-benzofuran-3(2H)-one; 1-(3-chloropropyl)pyrrolidine hydrochloride; With potassium carbonate; In acetone; Reflux;

With ethanol; acetyl chloride; at 0 - 20 ℃;

DOI:10.1016/j.bmc.2014.11.004

Reference yield:

(2Z)-6-hydroxy-2-(3-methoxybenzylidene)-1-benzofuran-3(2H)-one (1234351-88-2) + 1-(3-chloropropyl)piperidine hydrochloride (5472-49-1) → (Z)-2-(3-methoxybenzylidene)-6-(3-(piperidin-1-yl)propoxy)benzofuran-3(2H)-one hydrochloride

Guidance literature:

(2Z)-6-hydroxy-2-(3-methoxybenzylidene)-1-benzofuran-3(2H)-one; 1-(3-chloropropyl)piperidine hydrochloride; With potassium carbonate; In acetone; Reflux;

With ethanol; acetyl chloride; at 0 - 20 ℃;

DOI:10.1016/j.bmc.2014.11.004

upstream raw materials:

6-hydroxybenzofuran-3-one

3-methoxy-benzaldehyde

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