Technology Process of C29H25F4N7O2S
There total 7 articles about C29H25F4N7O2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium nitrite / acetic acid; water
2: sodium dithionite; ammonium hydroxide
3: water
4: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide
5: potassium carbonate / N,N-dimethyl-formamide
6: triethylamine / dichloromethane
7: dichloromethane
With
ammonium hydroxide; sodium dithionite; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium nitrite;
In
dichloromethane; water; acetic acid; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1248/cpb.c12-01046
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium dithionite; ammonium hydroxide
2: water
3: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide
4: potassium carbonate / N,N-dimethyl-formamide
5: triethylamine / dichloromethane
6: dichloromethane
With
ammonium hydroxide; sodium dithionite; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1248/cpb.c12-01046
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide
2: potassium carbonate / N,N-dimethyl-formamide
3: triethylamine / dichloromethane
4: dichloromethane
With
potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1248/cpb.c12-01046
