cis-(trimethylphosphine)(3,4-dimethyl-1-phenylphosphole)tetracarbonylmolybdenum

Base Information

Chemical Name:cis-(trimethylphosphine)(3,4-dimethyl-1-phenylphosphole)tetracarbonylmolybdenum
CAS No.:915297-83-5
Molecular Formula:C₁₉H₂₂MoO₄P₂
Molecular Weight:472.269
Hs Code.:

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Chemical Property of cis-(trimethylphosphine)(3,4-dimethyl-1-phenylphosphole)tetracarbonylmolybdenum

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Technology Process of cis-(trimethylphosphine)(3,4-dimethyl-1-phenylphosphole)tetracarbonylmolybdenum

There total 2 articles about cis-(trimethylphosphine)(3,4-dimethyl-1-phenylphosphole)tetracarbonylmolybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 16917-96-7
(trimethylphosphine)pentacarbonylmolybdenum

: 30540-36-4
3,4-dimethyl-1-phenylphosphole

: 915297-83-5
cis-(trimethylphosphine)(3,4-dimethyl-1-phenylphosphole)tetracarbonylmolybdenum

Guidance literature:: In tetrahydrofuran; Irradiation (UV/VIS); Mo-complex was dissolved in dry N2, N2 was bubbled through the soln., phosphole was added, the mixt. was stirred for 44 h while being irradiatedwith a high-pressure Hg-lamp; evapd. to dryness, column chromy. (silica gel, pentane/CH2Cl2 5:1), recrystd. from CH2Cl2/hexane;
DOI:10.1021/om060570t

Reference yield:

: 59967-36-1,65337-26-0
cis-tetracarbonylbis(piperidine)molybdenum

: 30540-36-4
3,4-dimethyl-1-phenylphosphole

: 594-09-2
trimethylphosphane

: 16027-45-5
cis-bis(trimethylphosphine)tetracarbonylmolybdenum

: 915297-83-5
cis-(trimethylphosphine)(3,4-dimethyl-1-phenylphosphole)tetracarbonylmolybdenum

Guidance literature:: DOI:10.1021/om060570t

Reference yield: 49.0%

: 915297-83-5
cis-(trimethylphosphine)(3,4-dimethyl-1-phenylphosphole)tetracarbonylmolybdenum

: 762-42-5
dimethyl acetylenedicarboxylate

: 915297-84-6
cis-(trimethylphosphine)(5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenylphosphanobornadiene)tetracarbonylmolybdenum

Guidance literature:: In neat (no solvent); (N2 atm.) a mixt. of complex and acetylene-compound was stirred for 22 hat 50°C; column chromy. (silica gel, pentane, pentane-CH2Cl2), recrystd. from CH2Cl2/hexane;
DOI:10.1021/om060570t