Technology Process of 6-<5-β-(N-methylamino)ethyl-2-methoxy>phenyloxyveratraldehyde
There total 6 articles about 6-<5-β-(N-methylamino)ethyl-2-methoxy>phenyloxyveratraldehyde which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 382 mg / LiAlH4 / tetrahydrofuran; diethyl ether / 1.) 20 min, RT, 2.) 50 deg C, 6 h
2: K2CO3 / CH2Cl2 / 1 h / Ambient temperature
3: 85 percent / H2 / 2percent PdCl2, C / methanol / 760 Torr
4: 49 percent / K2CO3, CuO, pyridine / 13 h / Heating
5: 171 mg / 10percent K2CO3 / methanol / 0.5 h / Heating
With
pyridine; lithium aluminium tetrahydride; hydrogen; potassium carbonate; copper(II) oxide;
palladium dichloride;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 89 percent / 6 h / Heating
2: 382 mg / LiAlH4 / tetrahydrofuran; diethyl ether / 1.) 20 min, RT, 2.) 50 deg C, 6 h
3: K2CO3 / CH2Cl2 / 1 h / Ambient temperature
4: 85 percent / H2 / 2percent PdCl2, C / methanol / 760 Torr
5: 49 percent / K2CO3, CuO, pyridine / 13 h / Heating
6: 171 mg / 10percent K2CO3 / methanol / 0.5 h / Heating
With
pyridine; lithium aluminium tetrahydride; hydrogen; potassium carbonate; copper(II) oxide;
palladium dichloride;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: K2CO3 / CH2Cl2 / 1 h / Ambient temperature
2: 85 percent / H2 / 2percent PdCl2, C / methanol / 760 Torr
3: 49 percent / K2CO3, CuO, pyridine / 13 h / Heating
4: 171 mg / 10percent K2CO3 / methanol / 0.5 h / Heating
With
pyridine; hydrogen; potassium carbonate; copper(II) oxide;
palladium dichloride;
In
methanol; dichloromethane;
