Technology Process of C17H19ClN2O2
There total 1 articles about C17H19ClN2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
tert-butyl (4-chloropyridin-3-yl)carbamate;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 0 ℃;
for 1.03333h;
Inert atmosphere;
Schlenk technique;
benzyl halide;
In
N,N-dimethyl-formamide; mineral oil;
at 0 - 20 ℃;
Inert atmosphere;
Schlenk technique;
DOI:10.1021/jo500064j
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
Inert atmosphere;
Schlenk technique;
DOI:10.1021/jo500064j
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere; Schlenk technique
2: potassium phosphate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex / tert-butyl alcohol / 4 h / 110 °C / Schlenk technique; Inert atmosphere
With
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; potassium phosphate; trifluoroacetic acid;
In
dichloromethane; tert-butyl alcohol;
DOI:10.1021/jo500064j