((C₆H₅)3PAu)2SO₄

Base Information

• Chemical Name: ((C₆H₅)3PAu)2SO₄
• CAS No.: 36539-10-3
• Molecular Formula: C₃₆H₃₀Au₂O₄P₂S
• Molecular Weight: 1014.58
• Mol file: 36539-10-3.mol

Synonyms:

Chemical Property of ((C₆H₅)3PAu)2SO₄

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of ((C₆H₅)3PAu)2SO₄

There total 2 articles about ((C₆H₅)3PAu)2SO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

(triphenylphosphine)gold(I) chloride (14243-64-2) + silver(I) acetate (563-63-3) → ((C6H5)3PAu)2SO4 (36539-10-3,24191-13-7)

Guidance literature:

With H₂SO₄; In methanol; benzene; byproducts: AgCl; Ph3PAuCl in C6H6 refluxed with CH3COOAg for 12 h, filtered, dried, dissolved in MeOH, H2SO4 added at 0°C; filtered with cooling, washed with H2O, dried, recrystd. from CH2Cl2/CH3OH; elem. anal.;

Reference yield:

2,4,6-trifluorophenyl(triphenylphosphine)gold(I) → ((C6H5)3PAu)2SO4 (36539-10-3,24191-13-7)

Guidance literature:

With H₂SO₄; In not given; byproducts: 1,3,5-C6F3H3; Au-complex reacted with H2SO4;

DOI:10.1016/S0022-328X(00)84690-2

upstream raw materials:

(triphenylphosphine)gold(I) chloride

silver(I) acetate