2-aminoethanethiolato(1-[2-(diphenylphosphino)phenyl]-2-methoxyethyl)gold(III) hexafluorophosphate * chloroform

Base Information

Chemical Name:2-aminoethanethiolato(1-[2-(diphenylphosphino)phenyl]-2-methoxyethyl)gold(III) hexafluorophosphate * chloroform
CAS No.:301153-35-5
Molecular Formula:CHCl₃*C₂₃H₂₆AuNOPS*F₆P
Molecular Weight:856.814
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-aminoethanethiolato(1-[2-(diphenylphosphino)phenyl]-2-methoxyethyl)gold(III) hexafluorophosphate * chloroform

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Technology Process of 2-aminoethanethiolato(1-[2-(diphenylphosphino)phenyl]-2-methoxyethyl)gold(III) hexafluorophosphate * chloroform

There total 2 articles about 2-aminoethanethiolato(1-[2-(diphenylphosphino)phenyl]-2-methoxyethyl)gold(III) hexafluorophosphate * chloroform which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: ammonium hexafluorophosphate

: 67-66-3,8013-54-5
chloroform

: 33896-43-4
dibromo(1-[2-(diphenylphosphino)phenyl]-2-methoxyethyl)gold(III)

: 156-57-0
2-mercaptoethylamine hydrochloride

: 301153-35-5
2-aminoethanethiolato(1-[2-(diphenylphosphino)phenyl]-2-methoxyethyl)gold(III) hexafluorophosphate * chloroform

Guidance literature:: With (C₂H₅)3N; In methanol; chloroform; MeOH solns. of ligand (3 molar equiv.) and Et3N mixed and added to CHCl3 soln. of Au complex, stirred for 15 min; solvent removed, residue washed (H2O), extd. (CHCl3), CHCl3 removed, residue dissolved in acetone, treated with NH4PF6/acetone, crystd.;
DOI:10.1039/b002248i