P,P-di(2-thiophenyl) phosphinamide

Base Information

• Chemical Name: P,P-di(2-thiophenyl) phosphinamide
• CAS No.: 315718-77-5
• Molecular Formula: C₈H₈NOPS₂
• Molecular Weight: 229.263
• Mol file: 315718-77-5.mol

Synonyms:

Chemical Property of P,P-di(2-thiophenyl) phosphinamide

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of P,P-di(2-thiophenyl) phosphinamide

There total 1 articles about P,P-di(2-thiophenyl) phosphinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

thiophen-2-yl magnesium bromide (5713-61-1) → tris(thiophen-2-yl)phosphine oxide (1021-21-2) + P,P-di(2-thiophenyl) phosphinamide (315718-77-5)

Guidance literature:

thiophen-2-yl magnesium bromide; With trichlorophosphate; In tetrahydrofuran; at 25 ℃; for 1h;

With ammonium hydroxide; In tetrahydrofuran; diethyl ether; at 0 ℃; for 1h; Further stages.;

DOI:10.1039/b311046j

Reference yield: 78.0%

cyclohexane (110-82-7,25012-93-5) + P,P-di(2-thiophenyl) phosphinamide (315718-77-5) → N-cyclohexyl-P,P-di(thiophen-2-yl)phosphinic amide

Guidance literature:

With copper(l) iodide; 1,10-Phenanthroline; bis(1-methyl-1-phenylethyl)peroxide; at 140 ℃; for 12h; Schlenk technique; Sealed tube; Molecular sieve;

DOI:10.1021/acs.joc.7b01527

upstream raw materials:

thiophen-2-yl magnesium bromide