(+/-)-6.7-Epi-aristolon

Base Information

Chemical Name:(+/-)-6.7-Epi-aristolon
CAS No.:3293-43-4
Molecular Formula:C₁₅H₂₂O
Molecular Weight:218.339
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-6.7-Epi-aristolon

Chemical Property:

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Technology Process of (+/-)-6.7-Epi-aristolon

There total 15 articles about (+/-)-6.7-Epi-aristolon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.7%

: 17334-55-3
β-gurjunene

: 3293-43-4,6831-17-0,20536-71-4,22419-46-1,25274-27-5,27779-52-8
aristolone

: 28398-06-3,808102-61-6
(1aR)-5-oxo-1.1.7c.7ac-tetramethyl-(1arH.7bcH)-1a.2.3.5.6.7.7a.7b-octahydro-1H-cyclopropa[a]naphthalene

: 26808-51-5
(1aR,3R,7R,7aR,7bS)-3-hydroxy-1,1,7,7a-tetramethyl-1,1a,2,3,6,7,7a,7b-octahydro-5H-cyclopropa[α]naphthalen-5-one

Guidance literature:: With culture medium of Chlorella fusca var. vacuocola IAMC-28; Noro medium; at 25 ℃; for 528h;
DOI:10.1248/cpb.54.861

Reference yield:

: 13395-76-1
2,3-dimethylcyclohexanone

: 3293-43-4,6831-17-0,20536-71-4,22419-46-1,25274-27-5,27779-52-8
(+/-)-Aristolon

Guidance literature:: Multi-step reaction with 6 steps

1: (i) NaOMe, (ii) /BRN= 906769/

2: TsOH

3: (i) KOtBu, (ii) aq. KOH

4: TsOH

5: (i) NaH, (ii) aq. KOH

With toluene-4-sulfonic acid;
DOI:10.1139/v69-132

Reference yield:

: 13395-76-1
2,3-dimethylcyclohexanone

: 3293-43-4,6831-17-0,20536-71-4,22419-46-1,25274-27-5,27779-52-8
(+/-)-6.7-Epi-aristolon

Guidance literature:: Multi-step reaction with 6 steps

1: (i) NaOMe, (ii) /BRN= 906769/

2: TsOH

3: (i) KOtBu, (ii) aq. KOH

4: TsOH

5: (i) NaH, (ii) aq. KOH

With toluene-4-sulfonic acid;
DOI:10.1139/v69-132