2-(dimethylphenylsiloxy)-2-butyl-1,2,3-oxazaborinane

Base Information

• Chemical Name: 2-(dimethylphenylsiloxy)-2-butyl-1,2,3-oxazaborinane
• CAS No.: 149694-02-0
• Molecular Formula: C₁₅H₂₈BNO₂Si
• Molecular Weight: 293.289
• Mol file: 149694-02-0.mol

Synonyms:

Chemical Property of 2-(dimethylphenylsiloxy)-2-butyl-1,2,3-oxazaborinane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2-(dimethylphenylsiloxy)-2-butyl-1,2,3-oxazaborinane

There total 1 articles about 2-(dimethylphenylsiloxy)-2-butyl-1,2,3-oxazaborinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

bis(dimethyl(phenyl)silyl) butylboronate (149834-95-7) + propan-1-ol-3-amine (156-87-6) → 2-(dimethylphenylsiloxy)-2-butyl-1,2,3-oxazaborinane (149694-02-0)

Guidance literature:

In dichloromethane; dropwise addn. of soln. of amine to a soln. of the B-compd. at room temp., stirring for 24 h; removal of solvent under vac. gives a liquid which is pumped in vac. overnight, addn. of ice-cold heptane, elem. anal.;

DOI:10.1016/S0277-5387(00)81537-5

upstream raw materials:

bis(dimethyl(phenyl)silyl) butylboronate

propan-1-ol-3-amine