BiO⁽¹⁺⁾*CH₃C₆H₄SO₃^(1-)=BiO(O₃SC₆H₄CH₃)

Base Information

Chemical Name:BiO⁽¹⁺⁾*CH₃C₆H₄SO₃^(1-)=BiO(O₃SC₆H₄CH₃)
CAS No.:108858-19-1
Molecular Formula:BiO*C₇H₇O₃S
Molecular Weight:396.177
Hs Code.:

BiO<sup>(1+)</sup>*CH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>SO<sub>3</sub><sup>(1-)</sup>=BiO(O<sub>3</sub>SC<sub>6</sub>H<sub>4</sub>CH<sub>3</sub>)

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Chemical Property of BiO⁽¹⁺⁾*CH₃C₆H₄SO₃^(1-)=BiO(O₃SC₆H₄CH₃)

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Technology Process of BiO⁽¹⁺⁾*CH₃C₆H₄SO₃^(1-)=BiO(O₃SC₆H₄CH₃)

There total 3 articles about BiO⁽¹⁺⁾*CH₃C₆H₄SO₃^(1-)=BiO(O₃SC₆H₄CH₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.8%

: 7446-11-9
sulfur trioxide

: 5142-75-6
tri(p-tolyl)bismuth

: 108858-15-7
di-p-tolylbismuth 4-methylbenzenesulfonate

: 108858-19-1
BiO⁽¹⁺⁾*CH₃C₆H₄SO₃^(1-)=BiO(O₃SC₆H₄CH₃)

: (p-tolyl)bismuth ditosylate

Guidance literature:: In 1,2-dichloro-ethane; bubbling SO3 through soln. of (CH3C6H4)3Bi in 1,2-dichloroethane for 2hat -10°C; pptn. on addn. of ether, filtn.; extn. with dry ethanol (insol. residue: BiO(O3SC6H4CH3); evapn. to dryness, major product: (p-MeC6H4)2Bi(O3Sp-MeC6H4), minor product: (p-MeC6H4)Bi(O3Sp-MeC6H4)2; elem. anal.;
DOI:10.1016/S0020-1693(00)86855-3

Reference yield:

: 108858-14-6
diphenylbismuth 4-methylbenzenesulfonate

: 108858-19-1
BiO⁽¹⁺⁾*CH₃C₆H₄SO₃^(1-)=BiO(O₃SC₆H₄CH₃)

Guidance literature:: With moisture; In neat (no solvent); byproducts: C6H6; decompn. on prolonged standing; elem. anal.; detn. by IR, (1)H-NMR;
DOI:10.1016/S0020-1693(00)86855-3

Reference yield:

: 1304-76-3
bismuth(III) oxide

: 104-15-4
toluene-4-sulfonic acid

: 108858-19-1
bismuth oxo(para-toluenesulphonate)

Guidance literature:: In neat (no solvent); excess of p-CH3C6H4SO3H; heating to 100°C for 4 to 6 h; completing react. at room temp. in 2-3 h; recovering of solids by stirring with diethyl ether; elem. anal.;