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1304-76-3

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1304-76-3 Usage

Chemical Properties

Heavy, Yellow Powder

Uses

In disinfectants, magnets, glass, rubber vulcanization; in fireproofing of papers and polymers; in catalysts.
InChI:InChI=1/4Bi.6O/rBi4O6/c5-1-6-3-8-2(5)9-4(7-1)10-3

1304-76-3 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Sigma-Aldrich (95381)  Bismuth(III)oxide  purum, ≥98.0% (KT) 1304-76-3 95381-500G 2,895.75CNY Detail
Sigma-Aldrich (95381)  Bismuth(III)oxide  purum, ≥98.0% (KT) 1304-76-3 95381-100G 811.98CNY Detail
Aldrich (223891)  Bismuth(III)oxide  ReagentPlus®, powder, 10 μm, 99.9% trace metals basis 1304-76-3 223891-500G 2,387.97CNY Detail
Aldrich (223891)  Bismuth(III)oxide  ReagentPlus®, powder, 10 μm, 99.9% trace metals basis 1304-76-3 223891-100G 686.79CNY Detail
Aldrich (202827)  Bismuth(III)oxide  powder, 99.999% trace metals basis 1304-76-3 202827-250G 4,626.18CNY Detail
Aldrich (202827)  Bismuth(III)oxide  powder, 99.999% trace metals basis 1304-76-3 202827-50G 1,668.42CNY Detail
Aldrich (202827)  Bismuth(III)oxide  powder, 99.999% trace metals basis 1304-76-3 202827-10G 542.88CNY Detail
Aldrich (637017)  Bismuth(III)oxide  nanopowder, 90-210 nm particle size, 99.8% trace metals basis 1304-76-3 637017-250G 4,449.51CNY Detail
Aldrich (637017)  Bismuth(III)oxide  nanopowder, 90-210 nm particle size, 99.8% trace metals basis 1304-76-3 637017-100G 2,354.04CNY Detail
Aldrich (637017)  Bismuth(III)oxide  nanopowder, 90-210 nm particle size, 99.8% trace metals basis 1304-76-3 637017-25G 810.81CNY Detail
Alfa Aesar (17132)  Bismuth(III) oxide, typically 99.99% (metals basis)    1304-76-3 250g 922.0CNY Detail
Alfa Aesar (17132)  Bismuth(III) oxide, typically 99.99% (metals basis)    1304-76-3 50g 378.0CNY Detail

1304-76-3SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name Bismuth trioxide

1.2 Other means of identification

Product number -
Other names Bismite

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:1304-76-3 SDS

1304-76-3Synthetic route

dimethyl-diphenyl-arsonium; tetraiodo bismuthate(III)

dimethyl-diphenyl-arsonium; tetraiodo bismuthate(III)

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
With ammonium hydroxide In ammonia hydrolysis on boiling in 0.5n NH4OH solution;;100%
trimethyl-phenyl-arsonium; tetraiodo bismuthate(III)

trimethyl-phenyl-arsonium; tetraiodo bismuthate(III)

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
With ammonium hydroxide In ammonia hydrolysis on boiling in 0.5n NH4OH solution;;100%
dimethyl-di-p-tolyl-arsonium; tetraiodo bismuthate(III)

dimethyl-di-p-tolyl-arsonium; tetraiodo bismuthate(III)

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
With ammonium hydroxide In ammonia hydrolysis on boiling in 0.5n NH4OH solution;;100%
methyl-tri-p-tolyl-arsonium; tetraiodo bismuthate(III)

methyl-tri-p-tolyl-arsonium; tetraiodo bismuthate(III)

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
With ammonium hydroxide In ammonia hydrolysis on boiling in 0.5n NH4OH solution;;100%
trimethyl-p-tolyl-arsonium; tetraiodo bismuthate(III)

trimethyl-p-tolyl-arsonium; tetraiodo bismuthate(III)

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
With ammonium hydroxide In ammonia hydrolysis on boiling in 0.5n NH4OH solution;;100%
methyl-triphenyl-arsonium; tetraiodo bismuthate(III)

methyl-triphenyl-arsonium; tetraiodo bismuthate(III)

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
With ammonium hydroxide In further solvent(s) hydrolysis on heating in 0.5n NH4OH solution;;100%
bismuth(III) chloride

bismuth(III) chloride

sodium carbonate
497-19-8

sodium carbonate

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
In water at 90℃; for 0.5h;95%
bismuth(III) acetate oxide

bismuth(III) acetate oxide

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
In propan-1-ol at 200℃;
In neat (no solvent) byproducts: CH3COOH; formation of acetic acid and Bi2O3 on heating above 150°C;; Bi2O3 contaminated by metallic Bi;;
bismuth(III) sulfide

bismuth(III) sulfide

mercury(II) oxide

mercury(II) oxide

A

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

B

mercury sulfide

mercury sulfide

Conditions
ConditionsYield
reaction on surface between HgO and Bi2S3; 200°C, 2 h;
In neat (no solvent) heating at 200°C;;
reaction on surface between HgO and Bi2S3; 200°C, 2 h;
In neat (no solvent) heating at 200°C;;
bismuth(III) selenite

bismuth(III) selenite

A

selenium(IV) oxide
7446-08-4

selenium(IV) oxide

B

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
In neat (no solvent) Kinetics; isothermal heating of Bi selenite in open Pt crucible in N2 flow (25 cm**3/min), temp. interval of 723-923 K;
bismuth subcarbonate

bismuth subcarbonate

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
In neat (no solvent) calcination;;
In neat (no solvent) heating of (BiO)2CO3 above 308°C;;
glowing starting material;;
bismuth (III) nitrate pentahydrate

bismuth (III) nitrate pentahydrate

water
7732-18-5

water

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
With lysozyme In water High Pressure; hydrothermaly, at 160°C; HRTEM, SAED;
With sodium hydrate or nitric acid; Sb(O2CCH3)3 In not given High Pressure; addn. of Sb compd. to soln. of Bi compd., pH 5, 7, 9 (sodium hydrate or nitric acid), sealing, storage in autoclave; XRD;
With sodium hydrate or nitric acid; Sb2O3 In not given High Pressure; addn. of Sb2O3 to soln. of Bi compd., pH 9 (sodium hydrate or nitric acid), sealing, storage in autoclave; XRD;
With sodium tetrahydroborate; cetyltrimethylammonim bromide
at 140℃; for 17h; Autoclave; High pressure;
bismuth hydroxide

bismuth hydroxide

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
With alkali In not given boiling in excess of alkali;;> 99
With alkali In not given in excess of alkali at 70-80 °C;;
With alkali In not given Kinetics; reaction with alkaline solns. in the cold;;
In neat (no solvent) probably by dehydration at 100 °C;;
at 400℃; under 760.051 Torr; for 3h;
bismuth hydroxide

bismuth hydroxide

A

bismuth oxide

bismuth oxide

B

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
With chlorine In potassium hydroxide inlet of Cl2 into a suspension of Bi(OH)3 in boiling KOH gives mixture of Bi2O3 and Bi2O4 (not separarted);; content of Bi2O4 increases with increasing density of alkali soln. and excess related to Bi2O3 {3};;
With Cl2 In potassium hydroxide aq. KOH; inlet of Cl2 into a suspension of Bi(OH)3 in boiling KOH gives mixture of Bi2O3 and Bi2O4 (not separarted);; content of Bi2O4 increases with increasing density of alkali soln. and excess related to Bi2O3 {3};;
bismuth (III) nitrate pentahydrate

bismuth (III) nitrate pentahydrate

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
With citric acid In nitric acid Bi salt in aq.HNO3 treated with (HO(CH2CH2O)200H, citric acid and t-Oct-C6H4-(OCH2CH2)x, x=9-10 as surfactant, beated up for 3 h, dipped onto glass, dried to 100°C, heated at 60°C, kept for 1 h, heated at 450-600°C; XRD, XPS;
With air or oxygen In neat (no solvent) flame-spray synthesis from Bi(NO3)3*5H2O disolved in various mixtures: methanol/HNO3, ethanol/HNO3, methoxy-2-propanol/HNO3, ethoxy-ethanol/HNO3, propylene glycol propylether/HNO3, diethylene glycol monoethylether/HNO3; powder XRD;
In neat (no solvent) byproducts: H2O, NO(x); sample heating at 8 K/min in 1.8 l/h N2 flow up to ca. 450°C; TG, DTG, DTA;
bismuth (III) nitrate pentahydrate

bismuth (III) nitrate pentahydrate

A

bismuth
7440-69-9

bismuth

B

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
In nitric acid aq. HNO3; Electrolysis; Pt, Al, Au or indium-tin oxide electrodes, constant potential (e.g. -0.4V) and constant current, in the presence or absence of Na2EDTA, room te mp.; rinsing with H2O, drying in blowing air;A n/a
B 0%
tetrabutoxytitanium

tetrabutoxytitanium

bismuth (III) nitrate pentahydrate

bismuth (III) nitrate pentahydrate

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
With potassium hydroxide; dihydrogen peroxide In nitric acid High Pressure; soln. of Bi(NO3)3*5H2O in aq. HNO3; NH3 added to soln. of Ti(OBu)4 and ppt. dissolved in aq. HNO3/H2O2; solns. mixed with stirring and ppt. formed with adding NH3; ppt. washed with H2O and placed in autoclave (160°C 4-6 h) with KOH(4.5 M); products removed out, filtered, washed with water and dried at 70°C for 6 h; XRD;
bismuth(III) nitrate

bismuth(III) nitrate

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
MoO3-substrate was impregnated with Bi(NO3)3 soln.; dried at room temp. with stirring, dried at 413 K for 10 h, calcined at 773 K for 5 h in air;
With aluminum oxide In water Al2O3 placed into aq. soln. of Bi(NO3)32; evapd. at 110°C for 12 h under stirring; calcined at 400-500°C for 5 h; Bi2O3 deposited on Al2O3 obtained;
With potassium hydroxide In water Bi-nitrate is suspended in water; warming up, addition of solid KOH gives hydroxide which reacts to the oxide above 70 °C;; filtrated ppt. is washed with hot water, dried with absol. alcohol or in desiccator at 250 °C;;
bismuth(III) nitrate

bismuth(III) nitrate

potassium hydroxide

potassium hydroxide

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
In water by pptn. of 1 M Bi(NO3)3 soln. in 1 M KOH at room temp.; purifn.: solid filterd, washed with distd. H2O and dried at 80°C;detd. by XRD;
bismuth(III) nitrate

bismuth(III) nitrate

ammonium hydroxide

ammonium hydroxide

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
pptn. from hot acidic soln. of Bi(III) nitrate with 1 mol dm**-3 NH4OH;
With HNO3 In water Bi(NO3)3 dissolved in dilute HNO3, dilute soln. of NH4OH added until pH=12; filtered, washed (H2O), fired at 600°C for 8 h;
Bi6Zn4Sb2O18

Bi6Zn4Sb2O18

zinc(II) oxide

zinc(II) oxide

A

zinc antimony spinel

zinc antimony spinel

B

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
reaction above 1300 K;
bismuth
7440-69-9

bismuth

tellurium(IV) oxide
7446-07-3

tellurium(IV) oxide

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
In neat (no solvent) addition of Bi to TeO2;;
byproducts: Te; moderate reaction;;
byproducts: Te; moderate reaction;;
In neat (no solvent) addition of Bi to TeO2;;
potassium barium bismuthate hydrate

potassium barium bismuthate hydrate

A

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

B

barium(II) oxide

barium(II) oxide

C

potassium oxide

potassium oxide

Conditions
ConditionsYield
thermal decompn. at 400°C; XRD;
bismuth oxide

bismuth oxide

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
With carbon monoxide In neat (no solvent) heating in a stream of CO at 245-250 °C;;
With oxygen In neat (no solvent) heating in O2-stream above 300 °C;;
With air In neat (no solvent) heating in air-stream above 300 °C;;
bismuth
7440-69-9

bismuth

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
In melt addition of W in presence of 2 at. % U into molten Bi at 1000°C, 4 hours; formation of Bi2O3;;
anodic (0.6 V versus SCE) or thermal oxidn.;
With Fehlings solution; In water boiling;;
bismuth
7440-69-9

bismuth

nitrogen(II) oxide
10102-43-9

nitrogen(II) oxide

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
400°C;
In not given heating to 400 °C;;
In not given heating to 400 °C;;
bismuth
7440-69-9

bismuth

oxygen
80937-33-3

oxygen

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
In neat (no solvent) vaporisation of 99.9 % Bi, 1E-5 torr, deposition on quartz glass and oxidation in a stream of O2 at 100°C;; thin layer;;
In neat (no solvent) Electrochem. Process; cathodic pulverization of Bi under O2 and condensation;; thin layer;;
In neat (no solvent) Electrochem. Process; cathodic pulverization of Bi under O2/Ar and condensation; cathodic current density 1.5 mA/cm*cm;; thin layer, condensation of 6.7 Å/sec;;
bismuth
7440-69-9

bismuth

dihydrogen peroxide
7722-84-1

dihydrogen peroxide

A

bismuth(V) oxide

bismuth(V) oxide

B

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
formation of a thin, brown layer;;
In neat (no solvent) byproducts: ozone; powdered Bi reacts vigorously with 100 % H2O2 after short time, sometimes under explosion and glowing of Bi; gas evolution;;A 0%
B n/a
In neat (no solvent) byproducts: ozone; powdered Bi reacts vigorously with 100 % H2O2 after short time, sometimes under explosion and glowing of Bi; gas evolution;;A 0%
B n/a
formation of a thin, brown layer;;
bismuth(III) chloride * nitrogen dioxide

bismuth(III) chloride * nitrogen dioxide

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
With water
In neat (no solvent) decomposition at weak heating;;
With H2O
In neat (no solvent) decomposition at weak heating;;
bismuth(II) oxide

bismuth(II) oxide

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
With air In neat (no solvent) heating of BiO in air;;
With potassium permanganate In water in alkaline soln.;;
With air In neat (no solvent) BiO smoulders during conversion on heating in air;;
bismuth(III) oxide
1304-76-3

bismuth(III) oxide

bismuth
7440-69-9

bismuth

Conditions
ConditionsYield
With zinc In neat (no solvent) byproducts: ZnO; complete reduction at 500°C;;100%
With Zn In neat (no solvent) byproducts: ZnO; complete reduction at 500°C;;100%
With urea byproducts: H2O, CO2, N2; react. in a crucible over a low Meker flame, heating gently for 10 min; metal was extd. manually with a spatula;71%
sulfur tetrafluoride
7783-60-0

sulfur tetrafluoride

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

bismuth(III) fluoride
7787-61-3

bismuth(III) fluoride

Conditions
ConditionsYield
In neat (no solvent) heating at 300°C;;100%
In neat (no solvent) heating Bi2O3 with SF4 at 300°C;;100%
In neat (no solvent) heating at 300°C;;100%
In neat (no solvent) heating Bi2O3 with SF4 at 300°C;;100%
addition of Bi2O3 to an excess of SF4;;
hydrogenchloride
7647-01-0

hydrogenchloride

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

bismuth(III) chloride
7787-60-2

bismuth(III) chloride

Conditions
ConditionsYield
In acetic acid byproducts: H2O;100%
In acetic acid byproducts: H2O;100%
In neat (no solvent) volatilization of Bi2O3 in HCl-stream at 130 °C;;> 99
In neat (no solvent) volatilization of Bi2O3 in HCl-stream at 130 °C;;> 99
In perchloric acid aq. HClO4; prepn. by dissolving Bi2O3 in 6 M HCl;
sodium oxide

sodium oxide

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

sodium bismutate

sodium bismutate

Conditions
ConditionsYield
With oxygen In neat (no solvent) heating of Na2O with Bi2O3 (at least 3mol : 1mol) in a dry stream of O2 at 650°C for 20 hours;;100%
With O2 In neat (no solvent) heating of Na2O with Bi2O3 (at least 3mol : 1mol) in a dry stream of O2 at 650°C for 20 hours;;100%
bismuth(III) oxide
1304-76-3

bismuth(III) oxide

salicylic acid
69-72-7

salicylic acid

Bi2O(4+)*4C6H4(OH)(COO)(1-)=Bi2O(C6H4(OH)CO2)4

Bi2O(4+)*4C6H4(OH)(COO)(1-)=Bi2O(C6H4(OH)CO2)4

Conditions
ConditionsYield
With KNO3; NH4NO3 In neat (no solvent, solid phase) mechanochemical synthesis: ion- and liquid-assistant grinding of Bi2O3:acid mixt. with 5% of ionic salt in stainless steel grinding jar with twostainless steel balls, mixt. ground for 30 min at 30 Hz, jar preheated to 80°C;100%
In water stoich. mixt. in water; detd. by XRD;
In neat (no solvent, solid phase) mechanochemical synthesis: liquid-assisted grinding of 1:2 mixt. of Bi2O3:acid in stainless steel grinding jar with two stainless steel balls, mixt. ground for 10-60 min at 30 Hz; detd. by XRD;
ammonium dihydrogen phosphate

ammonium dihydrogen phosphate

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

C4H6CoO4*4H2O

C4H6CoO4*4H2O

C4H6BaO4

C4H6BaO4

BaBi2CoP2O10

BaBi2CoP2O10

Conditions
ConditionsYield
at 299.84 - 1049.84℃; for 58h; Temperature;100%
(1S)-10-camphorsulfonic acid
3144-16-9

(1S)-10-camphorsulfonic acid

water
7732-18-5

water

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

[Bi18O12(OH)12(S-(+)-10-camphorsulfonate)18(H2O)2]*13H2O

[Bi18O12(OH)12(S-(+)-10-camphorsulfonate)18(H2O)2]*13H2O

Conditions
ConditionsYield
In not given99%
bismuth(III) oxide
1304-76-3

bismuth(III) oxide

4Bi(3+)*2HOCH2CH2O(1-)*5OCH2CH2O(2-)=Bi4C14H30O14

4Bi(3+)*2HOCH2CH2O(1-)*5OCH2CH2O(2-)=Bi4C14H30O14

Conditions
ConditionsYield
With ethylene glycol In ethylene glycol stirring of a suspension of Bi2O3 in boiling ethylene glycol for 40 minutes;; pptn.; filtration; washed with acetone and CHCl3; dried in vac.; elem. anal.;;98%
2-Picolinic acid
98-98-6

2-Picolinic acid

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

bismuth(III) 2-pyridine carboxylate

bismuth(III) 2-pyridine carboxylate

Conditions
ConditionsYield
In water soln. of the acid in H2O added to a suspn. of Bi2O3 in H2O, reflux, 48 h, until total consumption of the acid, mixt. cooled to room temp.; filtered, ppt. washed with H2O and EtOH, dried (vac.); elem. anal.;98%
Pyridine-2,6-dicarboxylic acid
499-83-2

Pyridine-2,6-dicarboxylic acid

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

{Bi(py-2-(COO)-6-(COOH))2}(OH)

{Bi(py-2-(COO)-6-(COOH))2}(OH)

Conditions
ConditionsYield
In water soln. of the acid in H2O added to a suspn. of Bi2O3 in H2O, reflux, 48 h, until total consumption of the acid, mixt. cooled to room temp.; filtered, ppt. washed with H2O and EtOH, dried (vac.); elem. anal.;98%
2-methyl-thiobenzoic acid
50684-47-4

2-methyl-thiobenzoic acid

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Bi(SOCC6H4CH3)3
220592-43-8

Bi(SOCC6H4CH3)3

Conditions
ConditionsYield
In dichloromethane stirring (35°C, 3-4 h); evapn., drying (vac.), recrystn. (acetone); elem. anal.;98%
hydrogen fluoride
7664-39-3

hydrogen fluoride

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

bismuth trifluoride

bismuth trifluoride

Conditions
ConditionsYield
In water at 20℃; for 1h;98%
2-Ethylhexanoic acid
149-57-5

2-Ethylhexanoic acid

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

bismuth(III) 2-ethylhexanoate

bismuth(III) 2-ethylhexanoate

Conditions
ConditionsYield
With acetic anhydride In acetic acid at 120 - 140℃;97.1%
trifluorormethanesulfonic acid
1493-13-6

trifluorormethanesulfonic acid

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

bismuth(lll) trifluoromethanesulfonate

bismuth(lll) trifluoromethanesulfonate

Conditions
ConditionsYield
In ethanol; water at 60℃; for 3h;97%
Pyridine-2,5-dicarboxylic acid
100-26-5

Pyridine-2,5-dicarboxylic acid

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

{Bi(py-2-(COO)-5-(COOH))2}(OH)

{Bi(py-2-(COO)-5-(COOH))2}(OH)

Conditions
ConditionsYield
In water Bi2O3 added to a soln. of the acid in hot H2O (80°C), mixt. stirred under reflux (110°C), 48 h; filtered, cooled, ppt. washed with hot H2O (80°C) and EtOH; elem. anal.;97%
bismuth(III) oxide
1304-76-3

bismuth(III) oxide

cesium iodide

cesium iodide

Cs3Bi2I9

Cs3Bi2I9

Conditions
ConditionsYield
Stage #1: bismuth(III) oxide With hydrogen iodide In water
Stage #2: cesium iodide In water
97%
potassium fluoride

potassium fluoride

hydrogen fluoride
7664-39-3

hydrogen fluoride

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

periodic acid
10450-60-9

periodic acid

KBi2(IO3)2F5

KBi2(IO3)2F5

Conditions
ConditionsYield
In water at 210℃; for 96h;97%
rubidium fluoride

rubidium fluoride

hydrogen fluoride
7664-39-3

hydrogen fluoride

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

periodic acid
10450-60-9

periodic acid

RbBi2(IO3)2F5

RbBi2(IO3)2F5

Conditions
ConditionsYield
In water at 210℃; for 96h;97%
glycolic Acid
79-14-1

glycolic Acid

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

2Bi(3+)*2OOCCH2O(2-)*O(2-)=Bi2C4H4O7

2Bi(3+)*2OOCCH2O(2-)*O(2-)=Bi2C4H4O7

Conditions
ConditionsYield
In water addn. of an aq. soln. of glycolic acid to a suspension of Bi2O3 in H2O; refluxing with stirring for 1 h;; pptn.; filtration; washed with H2O and acetone; elem. anal.;;96%
Pyridine-2,3-dicarboxylic acid
89-00-9

Pyridine-2,3-dicarboxylic acid

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

{Bi(py-2-(COO)-3-(COOH))2}(OH)

{Bi(py-2-(COO)-3-(COOH))2}(OH)

Conditions
ConditionsYield
In water soln. of the acid in H2O added to a suspn. of Bi2O3 in H2O, reflux, 48 h, until total consumption of the acid, mixt. cooled to room temp.; filtered, ppt. washed with H2O and EtOH, dried (vac.); elem. anal.;96%
2,3-dicarboxypyrazine
89-01-0

2,3-dicarboxypyrazine

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

{Bi(pz-2-(COO)-3-(COO))2}(OH)

{Bi(pz-2-(COO)-3-(COO))2}(OH)

Conditions
ConditionsYield
In water soln. of the acid in H2O added to a suspn. of Bi2O3 in H2O, reflux, 48 h, until total consumption of the acid, mixt. cooled to room temp.; filtered, ppt. washed with H2O and EtOH, dried (vac.); elem. anal.;96%
5-Methylsalicylic acid
89-56-5

5-Methylsalicylic acid

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

C6H3OHCH3COOBiO

C6H3OHCH3COOBiO

Conditions
ConditionsYield
In water; acetone refluxing (28 h); filtn., washing (water, acetone), drying (vac., P4O10, 24 h); elem. ana.;96%
acetic anhydride
108-24-7

acetic anhydride

bismuth(III) oxide
1304-76-3

bismuth(III) oxide

Conditions
ConditionsYield
In acetic anhydride; acetic acid byproducts: acetic acid; soln. of oxide in a mixt. of acetic anhydride (100 ml) and acetic acid (100 ml), refluxed (1.5 h), cooled (0°C), crystn.; filtration (Buechner funnel); elem. anal.;95%
refluxing starting material for 2h and crystallisation on cooling;;
bismuth(III) oxide
1304-76-3

bismuth(III) oxide

anthranilic acid
118-92-3

anthranilic acid

[(salN)Bi(μ-O)Bi(salN)]2Bi2O5

[(salN)Bi(μ-O)Bi(salN)]2Bi2O5

Conditions
ConditionsYield
In water; acetone refluxing (24 h); filtn., washing (water, acetone), drying (vac., P4O10, 24 h); elem. anal.;95%

1304-76-3Upstream product

1304-76-3Downstream Products

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