tris(2-chlorosulfenyl-1-phenyl-1,3-butanedionato)chromium(III)

Base Information

Chemical Name:tris(2-chlorosulfenyl-1-phenyl-1,3-butanedionato)chromium(III)
CAS No.:868743-79-7
Molecular Formula:C₃₀H₂₄Cl₃CrO₆S₃
Molecular Weight:735.07
Hs Code.:

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Chemical Property of tris(2-chlorosulfenyl-1-phenyl-1,3-butanedionato)chromium(III)

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Technology Process of tris(2-chlorosulfenyl-1-phenyl-1,3-butanedionato)chromium(III)

There total 2 articles about tris(2-chlorosulfenyl-1-phenyl-1,3-butanedionato)chromium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: tris(1,3-diphenyl-1,3-propanedionato)chromium(III)

: 10545-99-0
sulfur dichloride

: 868743-79-7
tris(2-chlorosulfenyl-1-phenyl-1,3-butanedionato)chromium(III)

Guidance literature:: In tetrahydrofuran; soln. SCl2 in THF was added dropwise at -10°C to stirred soln. complex in THF, mixt. was stirred for 40 min; solvent was evapd. in vac.; elem. anal.;
DOI:10.1007/s11176-005-0227-9

Reference yield: 70.0%

: tris(1-phenyl-1,3-butanedionato)chromium(III)

: 10545-99-0
sulfur dichloride

: 868743-79-7
tris(2-chlorosulfenyl-1-phenyl-1,3-butanedionato)chromium(III)

Guidance literature:: In hexane; SCl2 was added dropwise to stirred suspn. Cr complex in hexane, mixt. was stirred for 15 min; ppt. was filtered off, washed with hexane and vac.-dried; elem. anal.;
DOI:10.1007/s11176-005-0227-9