6-(3,4,5-trimethoxyphenyl)-6H-2,3,7,8-tetrahydrobenzo-1,3-thiazine-<2,3-b>quinazoline-3-one

Base Information

Chemical Name:6-(3,4,5-trimethoxyphenyl)-6H-2,3,7,8-tetrahydrobenzo-1,3-thiazine-<2,3-b>quinazoline-3-one
CAS No.:128483-45-4
Molecular Formula:C₂₄H₂₄N₂O₄S
Molecular Weight:436.532
Hs Code.:

6-(3,4,5-trimethoxyphenyl)-6H-2,3,7,8-tetrahydrobenzo<h>-1,3-thiazine-<2,3-b>quinazoline-3-one

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(3,4,5-trimethoxyphenyl)-6H-2,3,7,8-tetrahydrobenzo-1,3-thiazine-<2,3-b>quinazoline-3-one

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Technology Process of 6-(3,4,5-trimethoxyphenyl)-6H-2,3,7,8-tetrahydrobenzo-1,3-thiazine-<2,3-b>quinazoline-3-one

There total 4 articles about 6-(3,4,5-trimethoxyphenyl)-6H-2,3,7,8-tetrahydrobenzo-1,3-thiazine-<2,3-b>quinazoline-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 590-92-1
3-Bromopropionic acid

: 128483-28-3
2-Mercapto-4-(3,4,5-trimethoxyphenyl)-4H-1,2,3,4,5,6-hexahydrobenzo-quinazoline

: 128483-45-4
6-(3,4,5-trimethoxyphenyl)-6H-2,3,7,8-tetrahydrobenzo-1,3-thiazine-<2,3-b>quinazoline-3-one

Guidance literature:: With sodium acetate; acetic anhydride; In acetic acid; for 2h; Heating;

Reference yield:

: 128483-24-9
2-(3,4,5-trimethoxybenzylidene)-3,4-dihydronaphthalen-1(2H)-one

: 128483-45-4
6-(3,4,5-trimethoxyphenyl)-6H-2,3,7,8-tetrahydrobenzo-1,3-thiazine-<2,3-b>quinazoline-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / aq. KOH / ethanol / 0.5 h / Heating

2: 84 percent / CH₃COONa, (CH₃CO)2O / acetic acid / 2 h / Heating

With potassium hydroxide; sodium acetate; acetic anhydride; In ethanol; acetic acid;

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 128483-45-4
6-(3,4,5-trimethoxyphenyl)-6H-2,3,7,8-tetrahydrobenzo-1,3-thiazine-<2,3-b>quinazoline-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / 4percent KOH / ethanol / 0.08 h / Ambient temperature

2: 89 percent / aq. KOH / ethanol / 0.5 h / Heating

3: 84 percent / CH₃COONa, (CH₃CO)2O / acetic acid / 2 h / Heating

With potassium hydroxide; sodium acetate; acetic anhydride; In ethanol; acetic acid;