benzyl 2-thiazolyl ketone O-benzyloxime

Base Information

Chemical Name:benzyl 2-thiazolyl ketone O-benzyloxime
CAS No.:144775-02-0
Molecular Formula:C₁₈H₁₆N₂OS
Molecular Weight:308.404
Hs Code.:

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Chemical Property of benzyl 2-thiazolyl ketone O-benzyloxime

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Technology Process of benzyl 2-thiazolyl ketone O-benzyloxime

There total 3 articles about benzyl 2-thiazolyl ketone O-benzyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 144774-99-2
2-phenyl-1-(1,3-thiazol-2-yl)ethanone

: 144775-02-0,144775-03-1
benzyl 2-thiazolyl ketone O-benzyloxime

Guidance literature:: With pyridine; for 22h; Ambient temperature;
DOI:10.1016/S0040-4020(01)88264-8

Reference yield:

: 103-82-2
phenylacetic acid

: 144775-02-0,144775-03-1
benzyl 2-thiazolyl ketone O-benzyloxime

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / diethyl phosphorocyanidate (DEPC), NEt₃ / dimethylformamide / 1) -10 deg C, 0.5 h, 2) r.t., 2.5 h

2: 1) BuLi, N,N,N',N'-tetramethylethylenediamine (TMEDA) / 1) hexane, THF, -78 deg C, 2 h, 2a) THF, -78 deg C, 0.5 h, 2b) -10 deg C, 2 h

3: 82 percent / pyridine / 22 h / Ambient temperature

With pyridine; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)88264-8

Reference yield:

: 95092-10-7
N-methoxy-N-methyl-2-phenylacetamide

: 144775-02-0,144775-03-1
benzyl 2-thiazolyl ketone O-benzyloxime

Guidance literature:: Multi-step reaction with 2 steps

1: 1) BuLi, N,N,N',N'-tetramethylethylenediamine (TMEDA) / 1) hexane, THF, -78 deg C, 2 h, 2a) THF, -78 deg C, 0.5 h, 2b) -10 deg C, 2 h

2: 82 percent / pyridine / 22 h / Ambient temperature

With pyridine; n-butyllithium; N,N,N,N,-tetramethylethylenediamine;
DOI:10.1016/S0040-4020(01)88264-8