C₃₃H₃₂N₂O₈

Base Information

Chemical Name:C₃₃H₃₂N₂O₈
CAS No.:1160950-97-9
Molecular Formula:C₃₃H₃₂N₂O₈
Molecular Weight:584.626
Hs Code.:

C<sub>33</sub>H<sub>32</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:

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Chemical Property of C₃₃H₃₂N₂O₈

Chemical Property:

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Technology Process of C₃₃H₃₂N₂O₈

There total 10 articles about C₃₃H₃₂N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1083312-78-0
benzyl 7-hydroxy-6-methoxy-8-methyl-2-oxo-2H-chromen-3-ylcarbamate

: 1160950-97-9
C₃₃H₃₂N₂O₈

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine / 12 h

2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 12 h

3: triethylamine / tetrahydrofuran / 12 h

4: triethylamine / methanol / 12 h / 20 °C

5: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 0 °C

6: trifluoroacetic acid / dichloromethane / 12 h / 20 °C

7: pyridine

With di-isopropyl azodicarboxylate; palladium 10% on activated carbon; hydrogen; triethylamine; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; pyridine; methanol; dichloromethane; 5: Mitsunobu reaction;
DOI:10.1021/jm200148p

Reference yield:

: 1083313-05-6
3′,6-dimethoxy-[1,1′-biphenyl]-3-carboxylic acid

: 1160950-97-9
C₃₃H₃₂N₂O₈

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride / tetrahydrofuran

2: triethylamine / tetrahydrofuran / 12 h

3: triethylamine / methanol / 12 h / 20 °C

4: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 0 °C

5: trifluoroacetic acid / dichloromethane / 12 h / 20 °C

6: pyridine

With thionyl chloride; di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; pyridine; methanol; dichloromethane; 4: Mitsunobu reaction;
DOI:10.1021/jm200148p

Reference yield:

: 1083313-80-7
3',6-dimethoxy-[1,1'-biphenyl]-3-carbonyl chloride

: 1160950-97-9
C₃₃H₃₂N₂O₈

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / tetrahydrofuran / 12 h

2: triethylamine / methanol / 12 h / 20 °C

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 0 °C

4: trifluoroacetic acid / dichloromethane / 12 h / 20 °C

5: pyridine

With di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; pyridine; methanol; dichloromethane; 3: Mitsunobu reaction;
DOI:10.1021/jm200148p