N-benzylideneaminophenanthrene-9,10-dicarboximide

Base Information

Chemical Name:N-benzylideneaminophenanthrene-9,10-dicarboximide
CAS No.:81568-58-3
Molecular Formula:C₂₃H₁₄N₂O₂
Molecular Weight:350.376
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzylideneaminophenanthrene-9,10-dicarboximide

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Technology Process of N-benzylideneaminophenanthrene-9,10-dicarboximide

There total 7 articles about N-benzylideneaminophenanthrene-9,10-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 100-52-7
benzaldehyde

: 81573-51-5
N-aminophenanthrene-9,10-dicarboximide

: 81568-58-3
N-benzylideneaminophenanthrene-9,10-dicarboximide

Guidance literature:: With acetic acid; In ethanol; for 1h; Heating;

Reference yield:

: 883-20-5
9-methylphenanthrene

: 81568-58-3
N-benzylideneaminophenanthrene-9,10-dicarboximide

Guidance literature:: Multi-step reaction with 5 steps

1: 63 percent / stannic chloride / 1,2-dichloro-ethane / 24 h

2: sodium dichromate / H₂O / 18 h / 250 °C

3: 83 percent / acetic anhydride / Heating

4: 65 percent / hydrazine hydrate / ethanol / 6 h / Heating

5: 67 percent / acetic acid / ethanol / 1 h / Heating

With sodium dichromate; acetic anhydride; tin(IV) chloride; hydrazine hydrate; acetic acid; In ethanol; water; 1,2-dichloro-ethane;

Reference yield:

: 85-01-8
phenanthrene

: 81568-58-3
N-benzylideneaminophenanthrene-9,10-dicarboximide

Guidance literature:: Multi-step reaction with 7 steps

1: 43 percent / stannic chloride / 24 h / Ambient temperature

2: 95 percent / potassium hydroxide, hydrazine hydrate / various solvent(s) / 3 h / Heating

3: 63 percent / stannic chloride / 1,2-dichloro-ethane / 24 h

4: sodium dichromate / H₂O / 18 h / 250 °C

5: 83 percent / acetic anhydride / Heating

6: 65 percent / hydrazine hydrate / ethanol / 6 h / Heating

7: 67 percent / acetic acid / ethanol / 1 h / Heating

With potassium hydroxide; sodium dichromate; acetic anhydride; tin(IV) chloride; hydrazine hydrate; acetic acid; In ethanol; water; 1,2-dichloro-ethane;