oxovanadium(IV) (benzoate)(4-hydroxybenzoate)

Base Information

• Chemical Name: oxovanadium(IV) (benzoate)(4-hydroxybenzoate)
• CAS No.: 130565-59-2
• Molecular Formula: C₇H₅O₂*C₇H₅O₃*OV
• Molecular Weight: 325.171
• Mol file: 130565-59-2.mol

Synonyms:

Chemical Property of oxovanadium(IV) (benzoate)(4-hydroxybenzoate)

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of oxovanadium(IV) (benzoate)(4-hydroxybenzoate)

There total 1 articles about oxovanadium(IV) (benzoate)(4-hydroxybenzoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

sodium benzoate (532-32-1) + vanadyl(IV) sulfate hydrate + sodium 4-hydroxybenzoate (114-63-6) → oxovanadium(IV) (benzoate)(4-hydroxybenzoate) (130565-59-2)

Guidance literature:

In methanol; water; sodium hydroxybenzoate in water mixed with sodium benzoate in water, warmed (hot plate), dropwise addn. of VO(SO4) in 50% MeOH/H2O soln. with stirring, complex pptd. immediately; filtered, washed (hot 50% MeOH/H2O), dried (vac., anhyd. silica gel); elem. anal.;

upstream raw materials:

sodium benzoate

sodium 4-hydroxybenzoate