[3,5-Dimethoxy-2-(7-oxo-octanoyl)-phenyl]-acetic acid 2-oxo-1,2-diphenyl-ethyl ester

Base Information

Chemical Name:[3,5-Dimethoxy-2-(7-oxo-octanoyl)-phenyl]-acetic acid 2-oxo-1,2-diphenyl-ethyl ester
CAS No.:130684-89-8
Molecular Formula:C₃₂H₃₄O₇
Molecular Weight:530.618
Hs Code.:

Synonyms:

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Chemical Property of [3,5-Dimethoxy-2-(7-oxo-octanoyl)-phenyl]-acetic acid 2-oxo-1,2-diphenyl-ethyl ester

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Technology Process of [3,5-Dimethoxy-2-(7-oxo-octanoyl)-phenyl]-acetic acid 2-oxo-1,2-diphenyl-ethyl ester

There total 8 articles about [3,5-Dimethoxy-2-(7-oxo-octanoyl)-phenyl]-acetic acid 2-oxo-1,2-diphenyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36651-24-8
7,7-(ethylenedioxy)octan-1-ol

: 130684-89-8
[3,5-Dimethoxy-2-(7-oxo-octanoyl)-phenyl]-acetic acid 2-oxo-1,2-diphenyl-ethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 70 percent / pyridinium dichromate / CH₂Cl₂ / 10 h

2: 1) butyl-lithium / 1) ether, -78 deg C, 2) -78 deg C, 5 h

3: manganese dioxide / CH₂Cl₂ / 15 h

4: 38 percent / 100 h / 180 °C

5: 70 percent / pyridinium dichromate / dimethylformamide / 24 h

6: 150 mg / N,N'-dicyclohexylcarbodi-imide, DMAP / tetrahydrofuran / 12 h

With dmap; manganese(IV) oxide; dipyridinium dichromate; n-butyllithium; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 36651-18-0
ethyl 7,7-ethylenedioxyoctanoate

: 130684-89-8
[3,5-Dimethoxy-2-(7-oxo-octanoyl)-phenyl]-acetic acid 2-oxo-1,2-diphenyl-ethyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 93 percent / LAH / diethyl ether / 5 h

2: 70 percent / pyridinium dichromate / CH₂Cl₂ / 10 h

3: 1) butyl-lithium / 1) ether, -78 deg C, 2) -78 deg C, 5 h

4: manganese dioxide / CH₂Cl₂ / 15 h

5: 38 percent / 100 h / 180 °C

6: 70 percent / pyridinium dichromate / dimethylformamide / 24 h

7: 150 mg / N,N'-dicyclohexylcarbodi-imide, DMAP / tetrahydrofuran / 12 h

With dmap; manganese(IV) oxide; lithium aluminium tetrahydride; dipyridinium dichromate; n-butyllithium; dicyclohexyl-carbodiimide; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 36651-36-2
ethyl 7-oxaoctanoate

: 130684-89-8
[3,5-Dimethoxy-2-(7-oxo-octanoyl)-phenyl]-acetic acid 2-oxo-1,2-diphenyl-ethyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 81 percent / toluene-p-sulphonic acid / benzene / 15 h / Heating

2: 93 percent / LAH / diethyl ether / 5 h

3: 70 percent / pyridinium dichromate / CH₂Cl₂ / 10 h

4: 1) butyl-lithium / 1) ether, -78 deg C, 2) -78 deg C, 5 h

5: manganese dioxide / CH₂Cl₂ / 15 h

6: 38 percent / 100 h / 180 °C

7: 70 percent / pyridinium dichromate / dimethylformamide / 24 h

8: 150 mg / N,N'-dicyclohexylcarbodi-imide, DMAP / tetrahydrofuran / 12 h

With dmap; manganese(IV) oxide; lithium aluminium tetrahydride; dipyridinium dichromate; n-butyllithium; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; benzene;