2-(2-Methoxyethoxy)-1-phenylethanol

Base Information

• Chemical Name: 2-(2-Methoxyethoxy)-1-phenylethanol
• CAS No.: 6942-08-1
• Molecular Formula: C11H16 O3
• Molecular Weight: 196.246
• European Community (EC) Number: 834-973-5
• NSC Number: 57406
• DSSTox Substance ID: DTXSID40288729

Synonyms:2-(2-methoxyethoxy)-1-phenylethanol;6942-08-1;2-(2-METHOXYETHOXY)-1-PHENYLETHAN-1-OL;NSC57406;SCHEMBL12222364;DTXSID40288729;NSC-57406;AKOS011043691;CS-0222682;EN300-1122189

Chemical Property of 2-(2-Methoxyethoxy)-1-phenylethanol

Chemical Property:

• Vapor Pressure: 0.000451mmHg at 25°C
• Boiling Point: 302°C at 760 mmHg
• Flash Point: 136.4°C
• Density: 1.073g/cm³
• XLogP3: 0.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 6
• Exact Mass: 196.109944368
• Heavy Atom Count: 14
• Complexity: 133

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COCCOCC(C1=CC=CC=C1)O

Technology Process of 2-(2-Methoxyethoxy)-1-phenylethanol

There total 3 articles about 2-(2-Methoxyethoxy)-1-phenylethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

n-butyllithium (109-72-8,29786-93-4) + C4H9BrCl2O2Sn + benzaldehyde (100-52-7) → 1-Phenyl-1-pentanol (583-03-9) + α-[(2-methoxyethoxy)methyl]benzenemethanol (6942-08-1)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given; 1.) THF-hexane, 1 hr, -78 deg C, 2.) THF-hexane;

DOI:10.1016/S0040-4039(00)88124-1

Reference yield:

phenylmagnesium bromide (100-58-3) + 2-(2-methoxyethoxy)acetaldehyde (111964-99-9) → α-[(2-methoxyethoxy)methyl]benzenemethanol (6942-08-1)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1002/adsc.201000495

Reference yield:

→ α-[(2-methoxyethoxy)methyl]benzenemethanol (6942-08-1)

Guidance literature:

2-Brom-1-phenylethanol, 2-Methoxyethanol mit KOH;

upstream raw materials:

n-butyllithium

benzaldehyde

phenylmagnesium bromide

2-(2-methoxyethoxy)acetaldehyde

Downstream raw materials:

2-[2-(2-methoxyethoxy)-1-phenylethoxy]pyridine

4-[2-(2-methoxyethoxy)-1-phenylethoxy]pyridine

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