phenyldichloroacetoxygermane

Base Information

Chemical Name:phenyldichloroacetoxygermane
CAS No.:83686-66-2
Molecular Formula:C₈H₈Cl₂GeO₂
Molecular Weight:279.646
Hs Code.:

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Suppliers and Price of phenyldichloroacetoxygermane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyldichloroacetoxygermane

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Technology Process of phenyldichloroacetoxygermane

There total 2 articles about phenyldichloroacetoxygermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 623-73-4
diazoacetic acid ethyl ester

: 1074-29-9
trichlorophenylgermane

: 83686-66-2
phenyldichloroacetoxygermane

: 83686-67-3
GeClC₆H₅(O₂CCH₃)2

Guidance literature:: With acetic acid; In neat (no solvent); byproducts: ClCH2COOCH2CH3; 1 molar equiv of acetic acid adding to a mixt. of equimolar amts. of diazoacetate and chlorogermane; keeping for 24 h at 20°C; identified by gas chromy. and NMR spectrum;
DOI:10.1016/S0022-328X(00)87639-1

Reference yield:

: 1074-29-9
trichlorophenylgermane

: 83686-66-2
phenyldichloroacetoxygermane

Guidance literature:: With acetic acid; triethylamine; In benzene; byproducts: (CH3CH2)3NHCl; equimolar amts. of Ge deriv., AcOH and Et3N reacting for 2 h at ambienttemp., Et3NHCl filtering off, concg.; identified by NMR spectrum;
DOI:10.1016/S0022-328X(00)87639-1