2-Butyl-1-methylpyrrolidine

Base Information

• Chemical Name: 2-Butyl-1-methylpyrrolidine
• CAS No.: 3447-03-8
• Molecular Formula: C₉H₁₉N
• Molecular Weight: 141.257
• Mol file: 3447-03-8.mol

Synonyms:

Chemical Property of 2-Butyl-1-methylpyrrolidine

Chemical Property:

• Boiling Point: 40-41 °C(Press: 28 Torr)
• PKA: 10.62±0.40(Predicted)
• Density: 0.829±0.06 g/cm3(Predicted)

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Butyl-1-methylpyrrolidine

There total 6 articles about 2-Butyl-1-methylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-((Ξ)-butylidene)-1-methyl-pyrrolidine (99064-72-9) → pyrrolidine, 2-butyl-1-methyl- (3447-03-8)

Guidance literature:

With sulfuric acid; water; Bei der elektrochemischen Reduktion unter Verwendung einer Blei-Kathode;

DOI:10.1021/ja01333a052

Reference yield:

1-methyl-pyrrolidin-2-one (872-50-4,26138-58-9) → pyrrolidine, 2-butyl-1-methyl- (3447-03-8)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: Raney nickel; ethanol / Hydrogenation

With diethyl ether; ethanol; nickel;

DOI:10.1021/ja01263a020

Reference yield:

2-n-Butylpyrrolidine (3446-98-8) + formaldehyd (50-00-0,30525-89-4,61233-19-0) → pyrrolidine, 2-butyl-1-methyl- (3447-03-8)

Guidance literature:

With formic acid; at 115 - 130 ℃; im Rohr;

upstream raw materials:

2-n-Butylpyrrolidine

formaldehyd

2-((Ξ)-butylidene)-1-methyl-pyrrolidine

1-methyl-pyrrolidin-2-one